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Registro Completo |
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Biblioteca(s): |
Embrapa Agroindústria Tropical. |
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Data corrente: |
17/07/2025 |
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Data da última atualização: |
17/07/2025 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
SILVESTRE, F. A.; ANDRADE NETO, D. M.; ARAÚJO, A. C. R.; FERREIRA, M. A. DE A.; OLIVEIRA, D. L. V. DE; MARCIANO, S. J.; MATTOS, A. L. A.; MOREIRA, M. M.; FEITOSA, V. P.; PEIXOTO, R. F. |
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Afiliação: |
FRANCISBÊNIA ALVES SILVESTRE, FEDERAL UNIVERSITY OF CEARA; DAVINO MACHADO ANDRADE NETO, FEDERAL INSTITUTE OF EDUCATION, SCIENCE AND TECHNOLOGY OF CEARA; ÁLDRISON CANAFÍSTULA RÊGO ARAÚJO, FEDERAL INSTITUTE OF EDUCATION, SCIENCE AND TECHNOLOGY OF CEARA; MARCOS ANTONIO DE ALBUQUERQUE FERREIRA, FEDERAL INSTITUTE OF EDUCATION, SCIENCE AND TECHNOLOGY OF CEARA; DIEGO LOMONACO VASCONCELOS DE OLIVEIRA, FEDERAL UNIVERSITY OF CEARA; SARA JESSICA MARCIANO, FEDERAL UNIVERSITY OF CEARA; ADRIANO LINCOLN ALBUQUERQUE MATTOS, CNPAT; MADIANA MAGALHÃES MOREIRA, PAULO PICANÇO SCHOOL OF DENTISTRY; VICTOR PINHEIRO FEITOSA, UNIVERSITY OF IOWA; RANIEL FERNANDES PEIXOTO, FEDERAL UNIVERSITY OF CEARA. |
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Título: |
Evaluation of the physicochemical and adhesive properties of an etch-and-rinse adhesive system incorporated with magnesium whitlockite nanoparticles. |
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Ano de publicação: |
2025 |
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Fonte/Imprenta: |
Dental Materials, V. 41, N. 8, P. 938-946, 2025. |
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DOI: |
https://doi.org/10.1016/j.dental.2025.06.002 |
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Idioma: |
Inglês |
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Conteúdo: |
Objective: To synthesize and characterize magnesium whitlockite nanoparticles (nMg-WH) to evaluate the physicochemical and adhesive properties of a conventional adhesive incorporating different concentrations of nMg-WH. Method: nMg-WH were synthesized using a hydrothermal method and characterized using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Six groups of adhesive systems were prepared with different concentrations of nMg-WH (wt%: 0 % [Control], 0.1 %, 0.2 %, 0.5 %, 1 %, and 2 %) to evaluate the degree of conversion (DC, %), viscosity (cP), water sorption (WS, μg/mm³), and solubility (SL, μg/mm³). Forty-eight molars (n = 8) were sectioned and randomized between groups and evaluated for contact angle (in degrees) and microshear bond strength (μSBS), before and after thermocycling (TC) involving 10,000 cycles with a 30-s immersion time at temperatures of 5 ◦C and 55 ◦C. Statistical analysis was performed using one-way ANOVA (DC, cP, WS and SL) or mixed ANOVA (μSBS), followed by Tukey’s test for multiple comparisons (α = 0.05). Results: Regarding the physicochemical properties, the 0.2 % (51.3 ± 0.3), 0.5 % (49.0 ± 1.4), and 1 % (49.2 ± 1.9) nMg-WH groups showed significantly higher DC compared to the control (41.0 ± 0.2). The 0.2 % group presented the lowest contact angle (16.24 ± 7.79), indicating enhanced wettability. Viscosity increased proportionally with concentration, although 0.1 % (28.91 ± 0.75) remained comparable (p > 0.05) to the control (31.00 ± 1.08). WS and SL were not significantly affected at higher concentrations (0.5 %, 1 %, and 2 %). Before TC, the 0.1 % (32.1 ± 4.0) and 0.2 % (30.9 ± 2.1) nMg-WH groups demonstrated statistically higher (p < 0.05) μSBS values than the control (18.0 ± 5.2). After TC, concentrations of 0.2–2 % exhibited higher μSBS compared to the control, with the 0.5 % nMg-WH group showing the highest value (31.8 ± 1.0). Significance: nMg-WH improved the physicochemical properties of the adhesive system and increased adhesion to dentin, particularly at concentrations ranging from 0.2 % to 1 % MenosObjective: To synthesize and characterize magnesium whitlockite nanoparticles (nMg-WH) to evaluate the physicochemical and adhesive properties of a conventional adhesive incorporating different concentrations of nMg-WH. Method: nMg-WH were synthesized using a hydrothermal method and characterized using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Six groups of adhesive systems were prepared with different concentrations of nMg-WH (wt%: 0 % [Control], 0.1 %, 0.2 %, 0.5 %, 1 %, and 2 %) to evaluate the degree of conversion (DC, %), viscosity (cP), water sorption (WS, μg/mm³), and solubility (SL, μg/mm³). Forty-eight molars (n = 8) were sectioned and randomized between groups and evaluated for contact angle (in degrees) and microshear bond strength (μSBS), before and after thermocycling (TC) involving 10,000 cycles with a 30-s immersion time at temperatures of 5 ◦C and 55 ◦C. Statistical analysis was performed using one-way ANOVA (DC, cP, WS and SL) or mixed ANOVA (μSBS), followed by Tukey’s test for multiple comparisons (α = 0.05). Results: Regarding the physicochemical properties, the 0.2 % (51.3 ± 0.3), 0.5 % (49.0 ± 1.4), and 1 % (49.2 ± 1.9) nMg-WH groups showed significantly higher DC compared to the control (41.0 ± 0.2). The 0.2 % group presented the lowest contact angle (16.24 ± 7.79), indicating enhanced wettability. Viscosity increased proportionally with concentration, although 0.1 % (28.91 ± 0.7... Mostrar Tudo |
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Palavras-Chave: |
Chemical phenomena; Dentin-bonding agents; Magnesium whitlockite; Multifunctional nanoparticles. |
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Categoria do assunto: |
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Marc: |
LEADER 03144naa a2200289 a 4500
001 2177366
005 2025-07-17
008 2025 bl uuuu u00u1 u #d
024 7 $ahttps://doi.org/10.1016/j.dental.2025.06.002$2DOI
100 1 $aSILVESTRE, F. A.
245 $aEvaluation of the physicochemical and adhesive properties of an etch-and-rinse adhesive system incorporated with magnesium whitlockite nanoparticles.$h[electronic resource]
260 $c2025
520 $aObjective: To synthesize and characterize magnesium whitlockite nanoparticles (nMg-WH) to evaluate the physicochemical and adhesive properties of a conventional adhesive incorporating different concentrations of nMg-WH. Method: nMg-WH were synthesized using a hydrothermal method and characterized using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Six groups of adhesive systems were prepared with different concentrations of nMg-WH (wt%: 0 % [Control], 0.1 %, 0.2 %, 0.5 %, 1 %, and 2 %) to evaluate the degree of conversion (DC, %), viscosity (cP), water sorption (WS, μg/mm³), and solubility (SL, μg/mm³). Forty-eight molars (n = 8) were sectioned and randomized between groups and evaluated for contact angle (in degrees) and microshear bond strength (μSBS), before and after thermocycling (TC) involving 10,000 cycles with a 30-s immersion time at temperatures of 5 ◦C and 55 ◦C. Statistical analysis was performed using one-way ANOVA (DC, cP, WS and SL) or mixed ANOVA (μSBS), followed by Tukey’s test for multiple comparisons (α = 0.05). Results: Regarding the physicochemical properties, the 0.2 % (51.3 ± 0.3), 0.5 % (49.0 ± 1.4), and 1 % (49.2 ± 1.9) nMg-WH groups showed significantly higher DC compared to the control (41.0 ± 0.2). The 0.2 % group presented the lowest contact angle (16.24 ± 7.79), indicating enhanced wettability. Viscosity increased proportionally with concentration, although 0.1 % (28.91 ± 0.75) remained comparable (p > 0.05) to the control (31.00 ± 1.08). WS and SL were not significantly affected at higher concentrations (0.5 %, 1 %, and 2 %). Before TC, the 0.1 % (32.1 ± 4.0) and 0.2 % (30.9 ± 2.1) nMg-WH groups demonstrated statistically higher (p < 0.05) μSBS values than the control (18.0 ± 5.2). After TC, concentrations of 0.2–2 % exhibited higher μSBS compared to the control, with the 0.5 % nMg-WH group showing the highest value (31.8 ± 1.0). Significance: nMg-WH improved the physicochemical properties of the adhesive system and increased adhesion to dentin, particularly at concentrations ranging from 0.2 % to 1 %
653 $aChemical phenomena
653 $aDentin-bonding agents
653 $aMagnesium whitlockite
653 $aMultifunctional nanoparticles
700 1 $aANDRADE NETO, D. M.
700 1 $aARAÚJO, A. C. R.
700 1 $aFERREIRA, M. A. DE A.
700 1 $aOLIVEIRA, D. L. V. DE
700 1 $aMARCIANO, S. J.
700 1 $aMATTOS, A. L. A.
700 1 $aMOREIRA, M. M.
700 1 $aFEITOSA, V. P.
700 1 $aPEIXOTO, R. F.
773 $tDental Materials, V. 41, N. 8, P. 938-946, 2025.
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