02115naa a2200337 a 450000100080000000500110000800800410001902400390006010000220009924501260012126000090024752010750025665000230133165000220135465000200137665000310139665000090142765300320143665300330146865300280150165300190152965300200154865300200156870000230158870000210161170000200163270000180165270000260167070000180169677300630171421644902025-05-12       2025    bl uuuu     u00u1 u    #d7 a10.1080/14786419.2023.22720272DOI1 aMAGALHÃES, S. P.  aIdentification of volatile organic compounds in purple and white soybean flowers by HS-SPME/GC-MS.h[electronic resource]  c2025  aAbstract: This study aimed to establish a method for the extraction, enrichment, and identification of volatile organic compounds (VOCs) released by the flowers of purple (BRS 399) and white (DONMARIO 6563) soybean varieties. We tested the Static Headspace (HS) and Solid Phase Microextraction (SPME) methods using various fibre types: PDMS (Polydimethylsiloxane), PDMS/DVB (Divinylbenzene), and PDMS/DVB/CAR (Carboxen). We employed gas chromatography-mass spectrometry (GC-MS) to identify the VOCs. The SPME method with PDMS/DVB and PDMS/DVB/CAR fibres yielded the highest number of extracted compounds for both soybean cultivars. Notably, 67 compounds were detected in Glycine max. L for the first time. Using the developed method, we were able to detect 52 and 57 VOCs in the purple and white soybean varieties, respectively, including ketones, alcohols, aldehydes and benzenoids. In conclusion, the method we developed effectively identified VOCs in soybean flowers, thus enriching our understanding of the interactions between soybean flowers and their pollinators.  aGas chromatography  aMass spectrometry  aMicroextraction  aVolatile organic compounds  aSoja  aComposto orgânico volátil  aCromatografia em fase gasosa  aEspectrometria de massa  aFlores de soja  aMicroextração  aSoybean flowers1 aSILVA, J. M. G. da1 aGRAÇA, J. P. da1 aNUNES, E. de O.1 aZOCOLO, G. J.1 aHOFFMANN-CAMPO, C. B.1 aZERAIK, M. L.  tNatural Product Researchgv. 39, n. 7, p. 2006-2011, 2025.