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| Registros recuperados : 31 | |
| 2. |  | SENESI, G. S.; MARTIN NETO, L.; BOAS, P. R. V.; NICOLODELLI, G.; PEREIRA, D. M. B. Laser-based spectroscopic methods to evaluate the humification degree of soil organic matter in whole soils: a review Journal of Soils and Sediments, [S.l.], v. 18, n. 4, p. 1292-1302, 2016.| Biblioteca(s): Embrapa Instrumentação. |
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| 3. | | SENESI, G. S.; CARRARA, I.; NICOLODELLI, G.; MILORI, D. M. B. P.; PASCALE O. de. Laser cleaning and laser-induced breakdown spectroscopy applied in removing and characterizing black crusts from limestones of Castello Svevo, Bari, Italy: A case study Microchemical journal, [S. l.], v. 124, p. 296-305, 2016.| Biblioteca(s): Embrapa Instrumentação. |
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| 5. | | HUAMÁN, J. L. C.; TADINI, A. M.; SENESI, G. S.; MOUNIER, S.; MILORI, D. M. B. P.; NICOLODELLI, G. Characterization of an Amazon Soil Profile by Laser-Induced Breakdown, Raman, and Fluorescence Spectroscopies. Minerals, v. 13, 553, 2023. 9 p.| Biblioteca(s): Embrapa Instrumentação. |
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| 6. | | HUAMÁN, J. L. C.; NICOLODELLI, G.; SENESI, G. S.; MONTES, C. R.; PERRUCI, N. A. F.; BEZZON, V. D. N. Characterization and distribution of mineral phases in an Amazonian humiluvic Spodosol profile by XRPD, HR-TEM, SAED and SEM-EDX. Environmental Earth Sciences, v. 80, 405, 2021. 1 - 11| Biblioteca(s): Embrapa Instrumentação. |
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| 7. | | SENESI, G. S. NICOLODELLI, G. SANTOS, C. H. dos, MONTES, C.; VILLAS-BOAS, P. R.; MILORI, D. M. B. P. Espectroscopia de emissão óptica com plasma induzido por laser: um novo e versátil caminho para análise e monitoramento de solos, plantas e adubos. In: SIMPÓSIO NACIONAL DE INSTRUMENTAÇÃO AGROPECUÁRIA, 2014, São Carlos, SP Anais do SIAGRO: ciência, inovação e mercado 2014. São Carlos, SP: Embrapa Instrumentação, 2014. p. 325-328. Editores: Carlos Manoel Pedro Vaz, Débora Marcondes Bastos Pereira Milori, Silvio Crestana.| Biblioteca(s): Embrapa Instrumentação. |
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| 9. | | CLABEL HUAMÁN, J. L.; NICOLODELLI, G.; SENESI, G. S.; MONTES, C. R.; PERUCCI, N. A. F.; BEZZON, V. D. N.; MILORI, D. M. B. P. Characterization and distribution of mineral phases in an Amazonian humiluvic Spodosol profle by XRPD, HR_TEM, SAED and SEM_EDX. Environmental Earth Sciences, v. 80, n. 11, 2021. 1-11| Biblioteca(s): Embrapa Instrumentação. |
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| 10. | | RANULFI, A. C.; SENESI, G. S.; CAETANO, J. B.; MEYER, M. C.; MAGALHÃES, A. B.; BOAS, P. R. V.; MILORI, D. M. B. P. Nutritional characterization of healthy and Aphelenchoides besseyi infected soybean leaves by laser-induced breakdown spectroscopy (LIBS). Microchemical Journal, v. 141, p. 118-126, 2018.| Biblioteca(s): Embrapa Soja. |
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| 12. | | FERREIRA, E. C.; FERREIRA, E. J.; VILLAS-BOAS, P. R.; SENESI, G. S.; CARVALHO, C. M.; ROMANO, R. A.; MARTIN-NETO, L.; MILORI, D. M. B. P. Novel estimation of the humidification degree of soil organic matter by laser-induced breakdown spectroscopy. Spectrochimica Acta Part B, [S. l.], v. 99, p. 76-81, 2014.| Biblioteca(s): Embrapa Instrumentação. |
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| 13. | | CLABEL H, J. L.; NICOLODELLI, G.; SENESI, G. S.; MONTES, C. R.; PERRUCI, N. A. F.; BEZZON, V. D. N.; BALOGH, D. T.; MILORI, D. M. B. P. Organo-mineral associations in a Spodosol from northern Brazil. Geoderma Regional, v. 22, e00303, 2020.| Biblioteca(s): Embrapa Instrumentação. |
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| 14. | | NICOLODELLI, G.; VILLAS-BOAS, P. R.; MENEGATTI, C. R.; SENESI, G. S.; MAGALHÃES, D. V.; SOUZA, D. de; MILORI, D. M. B. P.; MARANGONI, B. S. Determination of Pb in soils by double-pulse laser-induced breakdown spectroscopy assisted by continuum wave-diode laser-induced fluorescence. Applied Optics, v. 57, n. 28, p. 8366-8372, out. 2018| Biblioteca(s): Embrapa Instrumentação. |
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| 15. | | NICOLODELLI, G.; SENESI, G. S.; RANULFI, A.; WATANABE, A.; CABRAL, J.; MARANGONI, B. S.; BOAS, P. R. V.; PEREIRA, D. M. B. Development of a Double-Pulse (DP) Laser-Induced Breakdown Spectroscopy (LIBS) Setup in the Orthogonal Configuration for Enviromental Applications. In: Latin América Optics and Photonics Conference 2016, Medellin, Colombia, Proceedings ... [S.l.:s.n.], 2016, não paginado.| Biblioteca(s): Embrapa Instrumentação. |
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| 16. | | MENEGATTI, C. R.; NICOLODELLI, G.; SENESI, G. S.; SILVA, O. A.; IFILHO, H. J.; VILLAS-BOAS, P. R.; MARANGONI, B. S.; MILORI, D. M. B. P. Evaluation of LIBS under controlled atmosphere to quantify cadmium at low concentration in landfill leachates. Applied Physics B, v. 125, a. 74, 2019. 1-6| Biblioteca(s): Embrapa Instrumentação. |
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| 17. | | NICOLODELLI, G.; SENESI, G. S.; PERAZZOLI, I. L. de O.; MARANGONI, B. S.; BENITES, V. de M.; MILORI, D. M. B. P. Double pulse laser induced breakdown spectroscopy: A potential tool for the analysis of contaminants and macro/micronutrients in organic mineral fertilizers. Science of the Total Environment, [S. l.], v. 565, p. 1116-1123, 2016.| Biblioteca(s): Embrapa Instrumentação; Embrapa Solos. |
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| 18. | | SENESI, G. S.; ROMANO, R. A.; MARANGONI, B. S.; NICOLODELLI, G.; BOAS, P. R. V.; BENITES, V. M.; MILORI, D. M. B. P. Laser-induced breakdown spectroscopy associated with multivariate analysis applied to discriminate fertilizers of different nature. In: Journal of Applied Spectroscopy, v. 84, n. 5, p. 923-928, 2017.| Biblioteca(s): Embrapa Instrumentação. |
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| 19. | | SENESI, G. S.; ROMANO, R. A.; MARANGONI, B. S.; NICOLODELLI, G.; VILLAS-BOAS, P. R.; BENITES, V. de M.; MILORI, D. M. B. P. Laser-induced breakdown spectroscopy associated with multivariate analysis applied to discriminate fertilizers of different nature. Journal of Applied Spectroscopy, v. 84, n. 5, p. 923-928, 2017.| Biblioteca(s): Embrapa Solos. |
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| 20. | | CERVANTES, C.; MARANGONI, B. S.; SENESI, G. S.; NICOLODELLI, G.; BOAS, P. R. V.; PEREIRA, D. M. B.; BENITES, V. de M. Quantificação e correção de matriz física de potássio em fertilizantes utilizando espectroscopia de emissão ótica com plasma induzido por laser (LIBS). In: JORNADA CIENTÍFICA - EMBRAPA SÃO CARLOS, 8., 2016, São Carlos, SP. Anais... São Carlos, SP: Embrapa Instrumentação: Embrapa Pecuária Sudeste, 2016. p. 20. (Embrapa Instrumentação. Documentos, 61).| Biblioteca(s): Embrapa Solos. |
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| Registros recuperados : 31 | |
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 | Acesso ao texto completo restrito à biblioteca da Embrapa Instrumentação. Para informações adicionais entre em contato com cnpdia.biblioteca@embrapa.br. |
Registro Completo
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Biblioteca(s): |
Embrapa Instrumentação. |
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Data corrente: |
06/04/2021 |
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Data da última atualização: |
10/06/2022 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 1 |
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Autoria: |
MARANGONI, B. S.; NICOLODELLI, G.; SENESI, G. S.; FONSECA, N.; IZARIO FILHO, H. J.; XAVIER, A. A.; VILLAS-BOAS, P. R.; MILORI, D. M. B. P.; MENEGATTI, C. R. |
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Afiliação: |
PAULINO RIBEIRO VILLAS BOAS, CNPDIA; DEBORA MARCONDES BASTOS PEREIRA, CNPDIA. |
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Título: |
Multi-elemental analysis of landfill leachates by single and double pulse laser-induced breakdown spectroscopy. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Microchemical Journal, v. 165, 106125, 2021. |
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ISSN: |
0026-265X |
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DOI: |
https://doi.org/10.1016/j.microc.2021.106125 |
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Idioma: |
Inglês |
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Conteúdo: |
In this work, the potential of single and double-pulse laser induced breakdown spectroscopy (SP and DP LIBS) has been investigated for multi-elemental analysis of the elements manganese, zinc, arsenic and lead in landfill leachates. Instrumental parameters such as detection delay and interpulse delay times were investigated in order to find the optimal operating values for multi-elemental analysis. The following emission lines were used: Mn II: 257.61; 259.37 and 260.56 nm; Zn II: 206.20 nm and Zn I: 213.85 nm; As I: 228.81; 234.98 nm and Pb I: 405.78 nm. All elements showed a strong enhancement factor (2.5) of DP LIBS signal intensities compared to SP LIBS. Analyses were performed using a background correction and the sum of the areas below each element emission lines. The limits of detection (LODs) achieved by SP LIBS were: 21.3, 77.5, 89.3, 38.9 mgkg− 1 and for DP LIBS: 7.1, 13.4, 11.9 and 7.3 mgkg− 1 respectively for Mn, Zn, As and Pb. The LOD values achieved by DP LIBS were improved by factors of 3, 6, 7.5 and 5 times respectively for Mn, Zn, As and Pb, with respect to SP LIBS. The average quantification errors were 7.5, 19.6, 38.2 and 28% for SP LIBS and 9.2, 21.3, 12.9 and 14.4% for DP LIBS respectively for Mn, Zn, As and Pb. The LIBS approach was demonstrated to be suitable for quantitative analysis of toxic elements and sufficiently fast for real time continuous monitoring of landfill leachates. |
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Palavras-Chave: |
Landfill leachate; LIBS; Mn; Zn. |
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Categoria do assunto: |
-- |
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Marc: |
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024 7 $ahttps://doi.org/10.1016/j.microc.2021.106125$2DOI
100 1 $aMARANGONI, B. S.
245 $aMulti-elemental analysis of landfill leachates by single and double pulse laser-induced breakdown spectroscopy.$h[electronic resource]
260 $c2021
520 $aIn this work, the potential of single and double-pulse laser induced breakdown spectroscopy (SP and DP LIBS) has been investigated for multi-elemental analysis of the elements manganese, zinc, arsenic and lead in landfill leachates. Instrumental parameters such as detection delay and interpulse delay times were investigated in order to find the optimal operating values for multi-elemental analysis. The following emission lines were used: Mn II: 257.61; 259.37 and 260.56 nm; Zn II: 206.20 nm and Zn I: 213.85 nm; As I: 228.81; 234.98 nm and Pb I: 405.78 nm. All elements showed a strong enhancement factor (2.5) of DP LIBS signal intensities compared to SP LIBS. Analyses were performed using a background correction and the sum of the areas below each element emission lines. The limits of detection (LODs) achieved by SP LIBS were: 21.3, 77.5, 89.3, 38.9 mgkg− 1 and for DP LIBS: 7.1, 13.4, 11.9 and 7.3 mgkg− 1 respectively for Mn, Zn, As and Pb. The LOD values achieved by DP LIBS were improved by factors of 3, 6, 7.5 and 5 times respectively for Mn, Zn, As and Pb, with respect to SP LIBS. The average quantification errors were 7.5, 19.6, 38.2 and 28% for SP LIBS and 9.2, 21.3, 12.9 and 14.4% for DP LIBS respectively for Mn, Zn, As and Pb. The LIBS approach was demonstrated to be suitable for quantitative analysis of toxic elements and sufficiently fast for real time continuous monitoring of landfill leachates.
653 $aLandfill leachate
653 $aLIBS
653 $aMn
653 $aZn
700 1 $aNICOLODELLI, G.
700 1 $aSENESI, G. S.
700 1 $aFONSECA, N.
700 1 $aIZARIO FILHO, H. J.
700 1 $aXAVIER, A. A.
700 1 $aVILLAS-BOAS, P. R.
700 1 $aMILORI, D. M. B. P.
700 1 $aMENEGATTI, C. R.
773 $tMicrochemical Journal$gv. 165, 106125, 2021.
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