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Registro Completo |
Biblioteca(s): |
Embrapa Instrumentação; Embrapa Solos. |
Data corrente: |
07/06/2016 |
Data da última atualização: |
28/06/2018 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Autoria: |
NICOLODELLI, G.; SENESI, G. S.; PERAZZOLI, I. L. de O.; MARANGONI, B. S.; BENITES, V. de M.; MILORI, D. M. B. P. |
Afiliação: |
DEBORA MARCONDES BASTOS PEREIRA, CNPDIA. |
Título: |
Double pulse laser induced breakdown spectroscopy: A potential tool for the analysis of contaminants and macro/micronutrients in organic mineral fertilizers. |
Ano de publicação: |
2016 |
Fonte/Imprenta: |
Science of the Total Environment, [S. l.], v. 565, p. 1116-1123, 2016. |
DOI: |
https://doi.org/10.1016/j.scitotenv.2016.05.153 |
Idioma: |
Inglês |
Conteúdo: |
Organic fertilizers are obtained from waste of plant or animal origin. One of the advantages of organic fertilizers is that, from the composting, it recycles waste-organic of urban and agriculture origin, whose disposal would cause environmental impacts. Fast and accurate analysis of both major and minor/trace elements contained in organic mineral and inorganic fertilizers of new generation have promoted the application of modern analytical techniques. In particular, laser induced breakdown spectroscopy (LIBS) is showing to be a very promising, quick and practical technique to detect and measure contaminants and nutrients in fertilizers. Although, this technique presents some limitations, such as a low sensitivity, if compared to other spectroscopic techniques, the use of double pulse (DP) LIBS is an alternative to the conventional LIBS in single pulse (SP). The macronutrients (Ca, Mg, K, P), micronutrients (Cu, Fe, Na, Mn, Zn) and contaminant (Cr) in fertilizer using LIBS in SP and DP configurations were evaluated. A comparative study for both configurations was performed using optimized key parameters for improving LIBS performance. The limit of detection (LOD) values obtained by DP LIBS increased up to seven times as compared to SP LIBS. In general, the marked improvement obtained when using DP system in the simultaneous LIBS quantitative determination for fertilizers analysis could be ascribed to the larger ablated mass of the sample. The results presented in this study show the promising potential of the DP LIBS technique for a qualitative analysis in fertilizers, without requiring sample preparation with chemical reagents. MenosOrganic fertilizers are obtained from waste of plant or animal origin. One of the advantages of organic fertilizers is that, from the composting, it recycles waste-organic of urban and agriculture origin, whose disposal would cause environmental impacts. Fast and accurate analysis of both major and minor/trace elements contained in organic mineral and inorganic fertilizers of new generation have promoted the application of modern analytical techniques. In particular, laser induced breakdown spectroscopy (LIBS) is showing to be a very promising, quick and practical technique to detect and measure contaminants and nutrients in fertilizers. Although, this technique presents some limitations, such as a low sensitivity, if compared to other spectroscopic techniques, the use of double pulse (DP) LIBS is an alternative to the conventional LIBS in single pulse (SP). The macronutrients (Ca, Mg, K, P), micronutrients (Cu, Fe, Na, Mn, Zn) and contaminant (Cr) in fertilizer using LIBS in SP and DP configurations were evaluated. A comparative study for both configurations was performed using optimized key parameters for improving LIBS performance. The limit of detection (LOD) values obtained by DP LIBS increased up to seven times as compared to SP LIBS. In general, the marked improvement obtained when using DP system in the simultaneous LIBS quantitative determination for fertilizers analysis could be ascribed to the larger ablated mass of the sample. The results presented in this study ... Mostrar Tudo |
Palavras-Chave: |
Fertilizante orgânico; Limite de detecção. |
Thesagro: |
Adubo Orgânico; Resíduo Orgânico. |
Categoria do assunto: |
-- P Recursos Naturais, Ciências Ambientais e da Terra |
Marc: |
LEADER 02516naa a2200241 a 4500 001 2063625 005 2018-06-28 008 2016 bl uuuu u00u1 u #d 024 7 $ahttps://doi.org/10.1016/j.scitotenv.2016.05.153$2DOI 100 1 $aNICOLODELLI, G. 245 $aDouble pulse laser induced breakdown spectroscopy$bA potential tool for the analysis of contaminants and macro/micronutrients in organic mineral fertilizers.$h[electronic resource] 260 $c2016 520 $aOrganic fertilizers are obtained from waste of plant or animal origin. One of the advantages of organic fertilizers is that, from the composting, it recycles waste-organic of urban and agriculture origin, whose disposal would cause environmental impacts. Fast and accurate analysis of both major and minor/trace elements contained in organic mineral and inorganic fertilizers of new generation have promoted the application of modern analytical techniques. In particular, laser induced breakdown spectroscopy (LIBS) is showing to be a very promising, quick and practical technique to detect and measure contaminants and nutrients in fertilizers. Although, this technique presents some limitations, such as a low sensitivity, if compared to other spectroscopic techniques, the use of double pulse (DP) LIBS is an alternative to the conventional LIBS in single pulse (SP). The macronutrients (Ca, Mg, K, P), micronutrients (Cu, Fe, Na, Mn, Zn) and contaminant (Cr) in fertilizer using LIBS in SP and DP configurations were evaluated. A comparative study for both configurations was performed using optimized key parameters for improving LIBS performance. The limit of detection (LOD) values obtained by DP LIBS increased up to seven times as compared to SP LIBS. In general, the marked improvement obtained when using DP system in the simultaneous LIBS quantitative determination for fertilizers analysis could be ascribed to the larger ablated mass of the sample. The results presented in this study show the promising potential of the DP LIBS technique for a qualitative analysis in fertilizers, without requiring sample preparation with chemical reagents. 650 $aAdubo Orgânico 650 $aResíduo Orgânico 653 $aFertilizante orgânico 653 $aLimite de detecção 700 1 $aSENESI, G. S. 700 1 $aPERAZZOLI, I. L. de O. 700 1 $aMARANGONI, B. S. 700 1 $aBENITES, V. de M. 700 1 $aMILORI, D. M. B. P. 773 $tScience of the Total Environment, [S. l.]$gv. 565, p. 1116-1123, 2016.
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1. | | DOMINGOS, D. F.; DELLAGNEZZE, B. M.; GREENFIELD, P.; REYES, L. R.; MELO, I. S. de; MIDGLEY, D. J.; OLIVEIRA, V. C. de. Draft genome sequence of the biosurfactant-producing bacterium Gordonia amicalis strain CCMA-559, isolated from petroleum-impacted sediment. Genome Announcements, Washington, DC, v. 1, n. 6, p. e00894-13, 2013.Tipo: Artigo em Periódico Indexado | Circulação/Nível: C - 0 |
Biblioteca(s): Embrapa Meio Ambiente. |
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2. | | DOMINGOS, D. F.; DELLAGNEZZE, B. M.; GREENFIELD, P.; REYES, L. F.; MELO, I. S. de; MIDGLEY, D. J.; OLIVEIRA, V. M. de. Draft genome sequence of Bacillus pumilus CCMA-560, isolated from an oil-contaminated mangrove swamp. Genome Announcements, Washington, DC, v. 1, n. 5, p. e00707-13, 2013.Tipo: Artigo em Periódico Indexado | Circulação/Nível: C - 0 |
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