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63. | ![Imagem marcado/desmarcado](/consulta/web/img/desmarcado.png) | RAIJ, B. V.; BORKERT, C. M.; OLIVEIRA JÚNIOR, A. Soil fertility management for soybean in Brazil. In: WORLD SOYBEAN RESEARCH CONFERENCE, 7.; INTERNATIONAL SOYBEAN PROCESSING AND UTILIZATION CONFERENCE, 4.; CONGRESSO BRASILEIRO DE SOJA, 3., 2004, Foz do Iguassu. Proceedings... Londrina: Embrapa Soybean, 2004. p. 407-414. Editado por Flávio Moscardi, Clara Beatriz Hoffmann-Campo, Odilon Ferreira Saraiva, Paulo Roberto Galerani, Francisco Carlos Krzyzanowski, Mercedes Concordia Carrão-Panizzi. Biblioteca(s): Embrapa Soja. |
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64. | ![Imagem marcado/desmarcado](/consulta/web/img/desmarcado.png) | BORKERT, C. M.; KLEPKER, D.; OLIVEIRA JUNIOR, A. de. Soybean response and residual effect of micronutrients in Cerrado soils. In: WORLD SOYBEAN RESEARCH CONFERENCE, 7.; INTERNATIONAL SOYBEAN PROCESSING AND UTILIZATION CONFERENCE, 4.; CONGRESSO BRASILEIRO DE SOJA, 3., 2004, Foz do Iguassu. Abstracts of contributed papers and posters. Londrina: Embrapa Soybean, 2004. p. 185-186. (Embrapa Soja. Documentos, 228). Editado por Flávio Moscardi, Clara Beatriz Hoffmann-Campo, Odilon Ferreira Saraiva, Paulo Roberto Galerani, Francisco Carlos Krzyzanowski, Mercedes Concordia Carrão-Panizzi. Biblioteca(s): Embrapa Soja. |
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71. | ![Imagem marcado/desmarcado](/consulta/web/img/desmarcado.png) | GIANLUPPI, D.; SMIDERLE, O, J.; GIANLUPPI, V.; BORKERT, C. M. Efeito da aplicação de doses de Zn a lanço sobre a produtividade de soja nos cerrados de Roraima nos dois primeiros cultivos. In: REUNIÃO DE PESQUISA DE SOJA DA REGIÃO CENTRAL DO BRASIL, 24., 2002, São Pedro, SP. Resumos... Londrina: Embrapa Soja, 2002. p. 109. (Embrapa Soja. Documentos, 185). Biblioteca(s): Embrapa Soja. |
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76. | ![Imagem marcado/desmarcado](/consulta/web/img/desmarcado.png) | SFREDO, G. J.; BORKERT, C. M.; PEREIRA, L. R. Cobre disponível para a cultura da soja, em dois solos do Paraná. In: CONGRESSO BRASILEIRO DE SOJA, 2.; MERCOSOJA 2002, 2002, Foz do Iguaçu. Perspectivas do agronegócio da soja: resumos. Londrina: Embrapa Soja, 2002. p. 220. (Embrapa Soja. Documentos, 181). Organizado por Odilon Ferreira Saraiva, Clara Beatriz Hoffmann-Campo. Biblioteca(s): Embrapa Soja. |
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80. | ![Imagem marcado/desmarcado](/consulta/web/img/desmarcado.png) | SFREDO, G. J.; LANTMANN, A. F.; BORKERT, C. M. Na medida certa. Cultivar: grandes culturas, Pelotas, v.2, n.21, p.20,22,24-25, out. 2000. Biblioteca(s): Embrapa Soja. |
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![](/consulta/web/img/deny.png) | Acesso ao texto completo restrito à biblioteca da Embrapa Agroindústria de Alimentos. Para informações adicionais entre em contato com ctaa.biblioteca@embrapa.br. |
Registro Completo
Biblioteca(s): |
Embrapa Agroindústria de Alimentos. |
Data corrente: |
20/05/2020 |
Data da última atualização: |
24/08/2020 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 1 |
Autoria: |
ALBINO, R. da C.; SIMAS, R. C.; MARTINS, K. da S.; BIZZO, H. R.; SILVA, E. R. da; Dal SASSO, M. A.; SILVA, R. V. S. da; LEITÃO, S. G.; OLIVEIRA, D. R. de. |
Afiliação: |
Rayane da Cruz Albino, UFRJ; Rosineide Costa Simas, UFG; Karine da Silva Martins, UFRJ; HUMBERTO RIBEIRO BIZZO, CTAA; Eduardo Rodrigues da Silva, UFRJ; Marco Aurélio Dal Sasso, UFRJ; Raquel Vieira Santana da Silva, UFRJ; Suzana Guimarães Leitão, UFRJ; Danilo Ribeiro de Oliveira, UFRJ. |
Título: |
Differentiation of black and white pitch (Burseraceae) oleoresins: A mass spectrometry-based chemoethnotaxonomic study. |
Ano de publicação: |
2020 |
Fonte/Imprenta: |
Journal of Ethnopharmacology, v. 259, 112968, p. 1-20, 2020. |
DOI: |
https://doi.org/10.1016/j.jep.2020.112968 |
Idioma: |
Inglês |
Notas: |
112968. |
Conteúdo: |
thnopharmacological relevance:In thequilombolacommunities of the municipality of Oriximiná (Pará State,Brazil),Protiumspp. (Burseraceae) oleoresins are distinguished in black and white pitch. White pitch oleoresinsmay be superior to black pitch in terms of quality, but the criteria used for their differentiation are fairlysubjective.Aim of the study:This study was designed to provide a scientific rationale for the traditional differentiation ofblack and white pitch oleoresins based on their non-volatile fraction.Materials and methods:Black and white pitch oleoresin samples collected inquilombolaterritories in Oriximináwere analysed by GC-EI-MS and UPLC-APCI-MS. The feasibility of EI and APCI mass spectrometry-based patternrecognition methods PLS-DA and Random Forest Analysis (RFA) for black and white pitch oleoresins differ-entiation was demonstrated.Results:The UPLC-APCI-MS method allowed the separation of 43 triterpenoids. Assessment of the triterpenoidfingerprints by GC-EI-MS led to the tentative identification of ursa-9(11),12-dien-3-ol as a potential marker forblack pitch oleoresins. PLS-DA and RFA applied to the APCI-MS and EI-MS data gave good models for black andwhite pitch oleoresins classification. The most important ions for the classifications of black pitch oleoresins byAPCI-MS/PLS-DA and APCI-MS/RFA likely represented triterpenoid acids.Conclusions:The triterpenoid pattern differs between black and white pitch oleoresins. The characteristic pre-sence of ursa-9(11),12-dien-3-ol and triterpenoids acids in black pitch oleoresins, along with otherfield ob-servations, suggest that black pitch oleoresins are actually aged white pitch oleoresins. Menosthnopharmacological relevance:In thequilombolacommunities of the municipality of Oriximiná (Pará State,Brazil),Protiumspp. (Burseraceae) oleoresins are distinguished in black and white pitch. White pitch oleoresinsmay be superior to black pitch in terms of quality, but the criteria used for their differentiation are fairlysubjective.Aim of the study:This study was designed to provide a scientific rationale for the traditional differentiation ofblack and white pitch oleoresins based on their non-volatile fraction.Materials and methods:Black and white pitch oleoresin samples collected inquilombolaterritories in Oriximináwere analysed by GC-EI-MS and UPLC-APCI-MS. The feasibility of EI and APCI mass spectrometry-based patternrecognition methods PLS-DA and Random Forest Analysis (RFA) for black and white pitch oleoresins differ-entiation was demonstrated.Results:The UPLC-APCI-MS method allowed the separation of 43 triterpenoids. Assessment of the triterpenoidfingerprints by GC-EI-MS led to the tentative identification of ursa-9(11),12-dien-3-ol as a potential marker forblack pitch oleoresins. PLS-DA and RFA applied to the APCI-MS and EI-MS data gave good models for black andwhite pitch oleoresins classification. The most important ions for the classifications of black pitch oleoresins byAPCI-MS/PLS-DA and APCI-MS/RFA likely represented triterpenoid acids.Conclusions:The triterpenoid pattern differs between black and white pitch oleoresins. The characteristic pre-sence of ursa-9(... Mostrar Tudo |
Palavras-Chave: |
Breu; Chemoethnotaxonomy; Espectrometria de massa; Plant resins; Quimioethnotaxonomia; Quimiometria; Resinas vegetais; Triterpenóides. |
Thesagro: |
Espectrometria; Oleorresina; Resina. |
Thesaurus NAL: |
Chemometrics; Triterpenoids. |
Categoria do assunto: |
F Plantas e Produtos de Origem Vegetal |
Marc: |
LEADER 02855naa a2200397 a 4500 001 2122419 005 2020-08-24 008 2020 bl uuuu u00u1 u #d 024 7 $ahttps://doi.org/10.1016/j.jep.2020.112968$2DOI 100 1 $aALBINO, R. da C. 245 $aDifferentiation of black and white pitch (Burseraceae) oleoresins$bA mass spectrometry-based chemoethnotaxonomic study.$h[electronic resource] 260 $c2020 500 $a112968. 520 $athnopharmacological relevance:In thequilombolacommunities of the municipality of Oriximiná (Pará State,Brazil),Protiumspp. (Burseraceae) oleoresins are distinguished in black and white pitch. White pitch oleoresinsmay be superior to black pitch in terms of quality, but the criteria used for their differentiation are fairlysubjective.Aim of the study:This study was designed to provide a scientific rationale for the traditional differentiation ofblack and white pitch oleoresins based on their non-volatile fraction.Materials and methods:Black and white pitch oleoresin samples collected inquilombolaterritories in Oriximináwere analysed by GC-EI-MS and UPLC-APCI-MS. The feasibility of EI and APCI mass spectrometry-based patternrecognition methods PLS-DA and Random Forest Analysis (RFA) for black and white pitch oleoresins differ-entiation was demonstrated.Results:The UPLC-APCI-MS method allowed the separation of 43 triterpenoids. Assessment of the triterpenoidfingerprints by GC-EI-MS led to the tentative identification of ursa-9(11),12-dien-3-ol as a potential marker forblack pitch oleoresins. PLS-DA and RFA applied to the APCI-MS and EI-MS data gave good models for black andwhite pitch oleoresins classification. The most important ions for the classifications of black pitch oleoresins byAPCI-MS/PLS-DA and APCI-MS/RFA likely represented triterpenoid acids.Conclusions:The triterpenoid pattern differs between black and white pitch oleoresins. The characteristic pre-sence of ursa-9(11),12-dien-3-ol and triterpenoids acids in black pitch oleoresins, along with otherfield ob-servations, suggest that black pitch oleoresins are actually aged white pitch oleoresins. 650 $aChemometrics 650 $aTriterpenoids 650 $aEspectrometria 650 $aOleorresina 650 $aResina 653 $aBreu 653 $aChemoethnotaxonomy 653 $aEspectrometria de massa 653 $aPlant resins 653 $aQuimioethnotaxonomia 653 $aQuimiometria 653 $aResinas vegetais 653 $aTriterpenóides 700 1 $aSIMAS, R. C. 700 1 $aMARTINS, K. da S. 700 1 $aBIZZO, H. R. 700 1 $aSILVA, E. R. da 700 1 $aDal SASSO, M. A. 700 1 $aSILVA, R. V. S. da 700 1 $aLEITÃO, S. G. 700 1 $aOLIVEIRA, D. R. de 773 $tJournal of Ethnopharmacology$gv. 259, 112968, p. 1-20, 2020.
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