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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
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Data corrente: |
25/11/2015 |
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Data da última atualização: |
15/03/2023 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
AMARAL, C. D. B.; AMAIS, R. S.; FIALHO, L. L.; SCHIAVO, D.; NOGUEIRA, A. R. de A.; NÓBREGA, J. A. |
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Afiliação: |
CLARICE D. B. AMARAL, UNIVERSIDADE FEDERAL DE SÃO CARLOS/SÃO CARLOS, SP; RENATA S. AMAIS, C CENTER FOR NUCLEAR ENERGY IN AGRICULTURE, UNIVERSITY OF SÃO PAULO, PIRACICABA, SP; LUCIMAR L. FIALHO, GROUP OF APPLIED INSTRUMENTAL ANALYSIS, DEPARTMENT OF CHEMISTRY, FEDERAL UNIVERSITY OF SÃO CARLOS; DANIELA SCHIAVO, Agilent Technologies Brazil; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; JOAQUIM A. NÓBREGA, GROUP OF APPLIED INSTRUMENTAL ANALYSIS, DEPARTMENT OF CHEMISTRY, FEDERAL UNIVERSITY OF SÃO CARLOS. |
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Título: |
Determination of carbon in digested samples and amino acids by inductively coupled plasma tandem mass spectrometry. |
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Ano de publicação: |
2015 |
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Fonte/Imprenta: |
Microchemical Journal, v. 122, n. 1, p. 29-32, 2015. |
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DOI: |
10.1016/j.microc.2015.04.007 |
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Idioma: |
Inglês |
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Conteúdo: |
Inductively coupled plasma mass spectrometer with a triple quadrupole (ICP-MS/MS) was employed to determine carbon from different sources such as plant digests, amino acids and peptides. Adequate precision, accuracy and sensitivity were obtained when using either single quadrupole or mass shift mode. Recoveries for carbon determination in plant digests ranged from 96 to 100%. Limits of detection were 0.42 and 0.17 mg L? 1 for 12C+ and 12C16O+, respectively, with calibration curves generated by using solutions prepared with oxalic acid. The determination of carbon and sulfur in amino acids and peptides showed that accuracy was better when measuring in O2 reaction mode. Additionally, C and S were simultaneously determined in cystine and glutathione by ICP-MS/MS mass-shift mode. The determination of carbon simultaneously with trace elements and target elements by ICP-MS makes this concept quite promising. Results demonstrated the potential of ICP-MS/MS for carbon determination. |
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Palavras-Chave: |
Amino acids Mass; Carbon determination; ICP MS MS; Non metal determination; Shift mode. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 01776naa a2200253 a 4500
001 2029454
005 2023-03-15
008 2015 bl uuuu u00u1 u #d
024 7 $a10.1016/j.microc.2015.04.007$2DOI
100 1 $aAMARAL, C. D. B.
245 $aDetermination of carbon in digested samples and amino acids by inductively coupled plasma tandem mass spectrometry.$h[electronic resource]
260 $c2015
520 $aInductively coupled plasma mass spectrometer with a triple quadrupole (ICP-MS/MS) was employed to determine carbon from different sources such as plant digests, amino acids and peptides. Adequate precision, accuracy and sensitivity were obtained when using either single quadrupole or mass shift mode. Recoveries for carbon determination in plant digests ranged from 96 to 100%. Limits of detection were 0.42 and 0.17 mg L? 1 for 12C+ and 12C16O+, respectively, with calibration curves generated by using solutions prepared with oxalic acid. The determination of carbon and sulfur in amino acids and peptides showed that accuracy was better when measuring in O2 reaction mode. Additionally, C and S were simultaneously determined in cystine and glutathione by ICP-MS/MS mass-shift mode. The determination of carbon simultaneously with trace elements and target elements by ICP-MS makes this concept quite promising. Results demonstrated the potential of ICP-MS/MS for carbon determination.
653 $aAmino acids Mass
653 $aCarbon determination
653 $aICP MS MS
653 $aNon metal determination
653 $aShift mode
700 1 $aAMAIS, R. S.
700 1 $aFIALHO, L. L.
700 1 $aSCHIAVO, D.
700 1 $aNOGUEIRA, A. R. de A.
700 1 $aNÓBREGA, J. A.
773 $tMicrochemical Journal$gv. 122, n. 1, p. 29-32, 2015.
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Registro original: |
Embrapa Pecuária Sudeste (CPPSE) |
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Registro Completo
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Biblioteca(s): |
Embrapa Rondônia. |
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Data corrente: |
16/09/2021 |
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Data da última atualização: |
16/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 2 |
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Autoria: |
MORAIS, J. A. de; ROCHA, R. B.; ALVES, E. A.; ESPINDULA, M. C.; TEIXEIRA, A. L.; SOUZA, C. A. de. |
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Afiliação: |
RODRIGO BARROS ROCHA, CPAF-RO; ENRIQUE ANASTACIO ALVES, CPAF-RO; MARCELO CURITIBA ESPINDULA, CPAF-RO; ALEXSANDRO LARA TEIXEIRA, CPAF-RO. |
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Título: |
Beverage quality of Coffea canephora genotypes in the western Amazon, Brazil. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Acta Scientiarum. Agronomy, v. 43, e52095, 2021. |
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ISSN: |
1807-8621 |
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DOI: |
10.4025/actasciagron.v43i1.52095 |
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Idioma: |
Inglês |
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Conteúdo: |
This study aimed to evaluate the beverage quality of Coffea canephora genotypes in different environments of the western Amazon to assist plant selection and new cultivar development. To analyze beverage quality, samples of cherry coffee beans were collected separately for each genotype from clonal competition trials installed in the municipalities of Ouro Preto do Oeste, Alta Floresta do Oeste, Porto Velho, and Ariquemes in Rondônia State and Rio Branco in Acre State (Brazil). The beverage quality was assessed using the Robusta Cupping Protocol, which attribute to each genotype a score in a range from 0 to 100, highlighting nuances. Analysis of variance and principal components using reference points were used to quantify genotype x environment interaction (G x E). The analysis of variance indicated that genotypic and G x E interaction effects were significant (p < 0.01). By using a centroid dispersion method, we could identify four clones of low, eight of specific (to favorable or unfavorable environments), and seven of broad adaptability to the environments. The clones BRS 2314, 11, and 17 had average quality scores above 80 in all environments, with potential for specialty coffee production. The clones BRS 1216, BRS 3220, and BRS 3193 presented unstable behavior, with beans of higher quality in some of the evaluated environments. Such inconsistency in clone behavior is caused by unpredictable changes in plant performance in different environments. Our results indicate that both genotypic (clones) and G x E interaction effects are important for the expression of coffee beverage quality. However, the clones BRS 3213, BRS 3210, and BRS 2299 had less prominent nuances, with lower potential for specialty coffee production. MenosThis study aimed to evaluate the beverage quality of Coffea canephora genotypes in different environments of the western Amazon to assist plant selection and new cultivar development. To analyze beverage quality, samples of cherry coffee beans were collected separately for each genotype from clonal competition trials installed in the municipalities of Ouro Preto do Oeste, Alta Floresta do Oeste, Porto Velho, and Ariquemes in Rondônia State and Rio Branco in Acre State (Brazil). The beverage quality was assessed using the Robusta Cupping Protocol, which attribute to each genotype a score in a range from 0 to 100, highlighting nuances. Analysis of variance and principal components using reference points were used to quantify genotype x environment interaction (G x E). The analysis of variance indicated that genotypic and G x E interaction effects were significant (p < 0.01). By using a centroid dispersion method, we could identify four clones of low, eight of specific (to favorable or unfavorable environments), and seven of broad adaptability to the environments. The clones BRS 2314, 11, and 17 had average quality scores above 80 in all environments, with potential for specialty coffee production. The clones BRS 1216, BRS 3220, and BRS 3193 presented unstable behavior, with beans of higher quality in some of the evaluated environments. Such inconsistency in clone behavior is caused by unpredictable changes in plant performance in different environments. Our results indicate th... Mostrar Tudo |
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Palavras-Chave: |
Conilon; Genotype x environments interaction; Robusta. |
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Categoria do assunto: |
-- |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/226081/1/8203Beverage-quality-of-Coffea-canephora-genotypes-in-the-western-Amazon-Brazil.pdf
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Marc: |
LEADER 02464naa a2200241 a 4500
001 2134468
005 2021-09-16
008 2021 bl uuuu u00u1 u #d
022 $a1807-8621
024 7 $a10.4025/actasciagron.v43i1.52095$2DOI
100 1 $aMORAIS, J. A. de
245 $aBeverage quality of Coffea canephora genotypes in the western Amazon, Brazil.$h[electronic resource]
260 $c2021
520 $aThis study aimed to evaluate the beverage quality of Coffea canephora genotypes in different environments of the western Amazon to assist plant selection and new cultivar development. To analyze beverage quality, samples of cherry coffee beans were collected separately for each genotype from clonal competition trials installed in the municipalities of Ouro Preto do Oeste, Alta Floresta do Oeste, Porto Velho, and Ariquemes in Rondônia State and Rio Branco in Acre State (Brazil). The beverage quality was assessed using the Robusta Cupping Protocol, which attribute to each genotype a score in a range from 0 to 100, highlighting nuances. Analysis of variance and principal components using reference points were used to quantify genotype x environment interaction (G x E). The analysis of variance indicated that genotypic and G x E interaction effects were significant (p < 0.01). By using a centroid dispersion method, we could identify four clones of low, eight of specific (to favorable or unfavorable environments), and seven of broad adaptability to the environments. The clones BRS 2314, 11, and 17 had average quality scores above 80 in all environments, with potential for specialty coffee production. The clones BRS 1216, BRS 3220, and BRS 3193 presented unstable behavior, with beans of higher quality in some of the evaluated environments. Such inconsistency in clone behavior is caused by unpredictable changes in plant performance in different environments. Our results indicate that both genotypic (clones) and G x E interaction effects are important for the expression of coffee beverage quality. However, the clones BRS 3213, BRS 3210, and BRS 2299 had less prominent nuances, with lower potential for specialty coffee production.
653 $aConilon
653 $aGenotype x environments interaction
653 $aRobusta
700 1 $aROCHA, R. B.
700 1 $aALVES, E. A.
700 1 $aESPINDULA, M. C.
700 1 $aTEIXEIRA, A. L.
700 1 $aSOUZA, C. A. de
773 $tActa Scientiarum. Agronomy$gv. 43, e52095, 2021.
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