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| Registros recuperados : 10 | |
| 2. |  | CASTRO, R. DE J. C.; SOUZA SOBRINHO, F. de; GAMA, M. A. S. da; BARRA, P. M. DE C.; ANTONIASSI, R.; OLIVEIRA, M. A. L. DE. Analysis of the main conjugated linoleic acid (CLA) precursors (C18:2 n-6 and C18:3 n-3) in Brachiaria ruzizienses by capillary zone electrophoresis. Central European Journal of Chemistry, v. 11, n. 8, p. 1286-1296, 2013. p. 1286-1296| Biblioteca(s): Embrapa Gado de Leite. |
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| 3. | | CASTRO, R. de J. C.; SOUZA SOBRINHO, F.; GAMA, M. A. S. da; BARRA, P. M. de C.; ANTONIASSI, R.; OLIVEIRA, M. A. L. de. Analysis of the main conjugated linoleic acid (CLA) precursors (C18:2 n-6 and C18:3 n-3) in Brachiaria ruzizienses by capillary zone electrophoresis. Central European Journal of Chemistry, v. 11, n. 8, p. 1286-1296, Aug. 2013.| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 4. | | CASTRO, R. DE J. C.; SOUZA SOBRINHO, F. de; GAMA, M. A. S. da; BARRA, P. M. DE C.; ANTONIASSI, R.; OLIVEIRA, M. A. L. DE. Simultaneous analysis of main fatty acids of CLA precursors in foraje by capillare zone electrophoresis. In: INTERNATIONAL SYMPOSIUM, EXHIBIT & WORKSHOPS ON ELECTRO- AND LIQUID PHASE-SEPARATION TECHNIQUES, 19., 2012, Baltimore. Book of abstracts. Stillwater: Oklahoma State University, 2012.| Biblioteca(s): Embrapa Gado de Leite. |
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| 5. | | CASTRO, R. DE J. C.; SATO, R. T.; SOUZA SOBRINHO, F. de; GAMA, M. A. S. da; OLIVEIRA, M. A. L. DE. Development of a rapid capillary zone electrophoresis method for the quantification of C18:2 N-6 and C18:3 N-3 fatty acids in forage samples. In: SIMPOSIO LATINOAMERICANO EN APLICACIONES DE LA ELECTROFORESIS CAPILAR Y TECNOLOGIA DEL MICROCHIP EN BIOTECNOLOGIA, BIOMEDICINA, BIOFARMACIA E INDUSTRIA, 18., 2012, Buenos Aires. Book of abstracts. Buenos Aires: [s.n.], 2012.| Biblioteca(s): Embrapa Gado de Leite. |
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| 6. | | RIBEIRO, C. G. S.; LOPES, F. C. F.; RODRIGUEZ, N. M.; GAMA, M. A. S. da; DORNELLAS, R. A. de C.; CASTRO, R. DE J. C. Parâmetros ruminais de vacas Holandês X Zebu em lactação alimentadas com dietas à base de capim-elefante picado contendo níveis crescentes de óleo de soja. In: REUNIÃO ANUAL DA SOCIEDADE BRASILEIRA DE ZOOTECNIA, 46., 2009, Maringá. Anais... Maringá: SBZ, 2009.| Biblioteca(s): Embrapa Gado de Leite. |
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| 7. | | CASTRO, R. de J. C.; SOUZA SOBRINHO, F. de; GAMA, M. A. S. da; SATO, R. T.; LIMA, L. L.; OLIVEIRA, M. A. L. de. A Rapid Method for Determination of the Main Conjugated Linoleic Acid Precursors (C18:2 n-6 and C18:3 n-3) in Forage by Capillary Zone Electrophoresis with Ultraviolet Detection Using Gas Chromatography with Flame Ionization Detection as a Comparative Method. Journal of AOAC International, v. 98, n. 6, p. 1591-1597, 2015.| Biblioteca(s): Embrapa Gado de Leite. |
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| 9. | | LOPES, F. C. F.; GAMA, M. A. S. da; ANTONIASSI, R.; BIZZO, H. R.; RIBEIRO, M. T.; RIBEIRO, C. G. dos S.; BARROS, P. A. V. de; CASTRO, R. de J. C.; MESQUITA, R. A. de; RODRIGUEZ, N. M. Índices de aterogenicidade e trombogenicidade de manteigas oriundas do leite de vacas consumindo dietas com óleo de soja. In: CONGRESSO BRASILEIRO DE CIÊNCIA E TECNOLOGIA DE ALIMENTOS, 21.; SEMINÁRIO LATINO AMERICANO E DO CARIBE DE CIÊNCIA E TECNOLOGIA DE ALIMENTOS, 15., 2008, Belo Horizonte. Ciência e inovação para o desenvolvimento sustentável. Belo Horizonte: SBCTA, 2008. 1 CD-ROM.| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 10. | | VIANA, J. H. M.; BATISTA, R. I. T. P.; RIBEIRO, C. A. S.; RAPOSO, N. R. B.; LOPES, F. C. F.; CASTRO, R. DE J. C.; CAMPOS, P. H. DE A.; OLIVEIRA, A. P.; GAMA, M. A. S. da. Correlation between fatty acids of follicular fluid from dairy cows fed tropical forage-based diets supplemented with increasing levels of soybean oil. In: ANNUAL MEETING OF THE EUROPEAN SOCIETY FOR PAEDIATRIC GASTROENTEROLOGY, HEPATOLOGY AND NUTRITION, 43., 2010, Istanbul. Abstracts... Ankara: Hacettepe University, 2010.| Biblioteca(s): Embrapa Gado de Leite. |
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| Registros recuperados : 10 | |
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Registro Completo
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Biblioteca(s): |
Embrapa Gado de Leite. |
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Data corrente: |
17/06/2013 |
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Data da última atualização: |
05/02/2024 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
B - 1 |
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Autoria: |
CASTRO, R. DE J. C.; SOUZA SOBRINHO, F. de; GAMA, M. A. S. da; BARRA, P. M. DE C.; ANTONIASSI, R.; OLIVEIRA, M. A. L. DE. |
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Afiliação: |
RENATA DE JESUS COELHO CASTRO, UFJF; FAUSTO DE SOUZA SOBRINHO, CNPGL; MARCO ANTONIO SUNDFELD DA GAMA, CNPGL; PATRICIA M. DE CASTRO BARRA, UFJF; ROSEMAR ANTONIASSI, CTAA; MARCONEI A. L. DE OLIVEIRA, UFJF. |
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Título: |
Analysis of the main conjugated linoleic acid (CLA) precursors (C18:2 n-6 and C18:3 n-3) in Brachiaria ruzizienses by capillary zone electrophoresis. |
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Ano de publicação: |
2013 |
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Fonte/Imprenta: |
Central European Journal of Chemistry, v. 11, n. 8, p. 1286-1296, 2013. |
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Páginas: |
p. 1286-1296 |
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Idioma: |
Inglês |
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Conteúdo: |
An alternative method for extraction optimization of C18:2 n-6 and C18:3 n-3, the main precursors for the synthesis of conjugated linoleic acid (CLA), in Brachiaria ruzizienses forages was proposed. Three methods of lipid extraction were tested: 1. Hara & Radin, 2. Micro Folch and 3. Bligh & Dyer. The preliminary test showed the Hara & Radin method as the most promising procedure. Then, a 33Box Behnken design with triplicate in the central point was applied in Hara & Radin method in order to optimize the extraction procedure. The optimization extraction was monitored by quantification of C18:2 n-6 and C18:3 n-3 through capillary zone electrophoresis (CZE). The results obtained by CZE were compared to gas chromatography (AOCS official method) in real samples using the paired t-test. No significant difference between methods was found within a 95% confidence interval (p-value= 0.937). The alternative CZE method for Brachiaria ruzizienses forages analysis has some advantages in comparison with official GC method such as, short analysis time (10 min), no derivatization step for sample preparation, absence of specific separation columns, lower analytical cost and high throughput. |
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Palavras-Chave: |
Desenho fatorial; Metodo de extração; Precurssor CLA. |
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Thesagro: |
Forragem. |
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Categoria do assunto: |
F Plantas e Produtos de Origem Vegetal |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/97936/1/Artigo-Fausto-Analysis-art3A10.24782Fs11532-013-0262-z.pdf
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Marc: |
LEADER 01998naa a2200241 a 4500
001 1959987
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008 2013 bl uuuu u00u1 u #d
100 1 $aCASTRO, R. DE J. C.
245 $aAnalysis of the main conjugated linoleic acid (CLA) precursors (C18$b2 n-6 and C18:3 n-3) in Brachiaria ruzizienses by capillary zone electrophoresis.$h[electronic resource]
260 $c2013
300 $ap. 1286-1296
520 $aAn alternative method for extraction optimization of C18:2 n-6 and C18:3 n-3, the main precursors for the synthesis of conjugated linoleic acid (CLA), in Brachiaria ruzizienses forages was proposed. Three methods of lipid extraction were tested: 1. Hara & Radin, 2. Micro Folch and 3. Bligh & Dyer. The preliminary test showed the Hara & Radin method as the most promising procedure. Then, a 33Box Behnken design with triplicate in the central point was applied in Hara & Radin method in order to optimize the extraction procedure. The optimization extraction was monitored by quantification of C18:2 n-6 and C18:3 n-3 through capillary zone electrophoresis (CZE). The results obtained by CZE were compared to gas chromatography (AOCS official method) in real samples using the paired t-test. No significant difference between methods was found within a 95% confidence interval (p-value= 0.937). The alternative CZE method for Brachiaria ruzizienses forages analysis has some advantages in comparison with official GC method such as, short analysis time (10 min), no derivatization step for sample preparation, absence of specific separation columns, lower analytical cost and high throughput.
650 $aForragem
653 $aDesenho fatorial
653 $aMetodo de extração
653 $aPrecurssor CLA
700 1 $aSOUZA SOBRINHO, F. de
700 1 $aGAMA, M. A. S. da
700 1 $aBARRA, P. M. DE C.
700 1 $aANTONIASSI, R.
700 1 $aOLIVEIRA, M. A. L. DE
773 $tCentral European Journal of Chemistry$gv. 11, n. 8, p. 1286-1296, 2013.
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Embrapa Gado de Leite (CNPGL) |
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