|
|
Registros recuperados : 324 | |
Registros recuperados : 324 | |
|
|
| Acesso ao texto completo restrito à biblioteca da Embrapa Alimentos e Territórios. Para informações adicionais entre em contato com mara.petrocchi@embrapa.br. |
Registro Completo
Biblioteca(s): |
Embrapa Alimentos e Territórios. |
Data corrente: |
17/11/2023 |
Data da última atualização: |
17/11/2023 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 2 |
Autoria: |
OIRAM FILHO, F.; MITRI, M. P.; ZOCOLO, G. J.; CANUTO, K. M.; BRITO, E. S. de. |
Afiliação: |
FRANCISCO OIRAM FILHO, Federal University of Ceará; MORGANA PEREIRA MITRI, Federal University of Ceará; GUILHERME JULIAO ZOCOLO, CNPAT; KIRLEY MARQUES CANUTO, CNPAT; EDY SOUSA DE BRITO, CNAT. |
Título: |
Validation of a method for anacardic acid quantification in cashew peduncles via high-performance liquid chromatography coupled to a diode-array detector. |
Ano de publicação: |
2023 |
Fonte/Imprenta: |
Foods, v. 12, n. 2759, 2023. |
Páginas: |
13 p. |
DOI: |
10.3390/foods12142759 |
Idioma: |
Inglês |
Conteúdo: |
The cashew peduncle has a high nutritional value and contains a wide variety of phenolic compounds. Among these, anacardic acids (AnAc) are biologically active components; however, they influence the cashew juice flavor and, consequently, its acceptance. This study validates a high-performance liquid chromatography method for quantifying the AnAc present in cashew peduncles, using a C18 reverse-phase column and a diode-array detector. The calibration curve obtained showed satisfactory precision for intraday (CV = 0.20%) and interday (CV = 0.29%) quantification, linearity (y = 2333.5x + 2956.2; r2 = 0.9979), repeatability with respect to retention time (CV = 0.45%) and area (CV = 0.30%), and selectivity, and possessed detection and quantification limits of 0.18 and 0.85 µg·mL?1, respectively. Different cashew clones containing AnAc were extracted and analyzed using the proposed method. A recovery of >90% was achieved using two sequential extractions. The total AnAc content ranged from 128.35 to 217.00 mg·100 g?1 in peduncle samples obtained from five different cashew clones. |
Palavras-Chave: |
Anacardic acid; HPLC; Validation. |
Thesagro: |
Anacardium Occidentale. |
Thesaurus NAL: |
Liquid chromatography. |
Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
Marc: |
LEADER 01868naa a2200253 a 4500 001 2158501 005 2023-11-17 008 2023 bl uuuu u00u1 u #d 024 7 $a10.3390/foods12142759$2DOI 100 1 $aOIRAM FILHO, F. 245 $aValidation of a method for anacardic acid quantification in cashew peduncles via high-performance liquid chromatography coupled to a diode-array detector.$h[electronic resource] 260 $c2023 300 $a13 p. 520 $aThe cashew peduncle has a high nutritional value and contains a wide variety of phenolic compounds. Among these, anacardic acids (AnAc) are biologically active components; however, they influence the cashew juice flavor and, consequently, its acceptance. This study validates a high-performance liquid chromatography method for quantifying the AnAc present in cashew peduncles, using a C18 reverse-phase column and a diode-array detector. The calibration curve obtained showed satisfactory precision for intraday (CV = 0.20%) and interday (CV = 0.29%) quantification, linearity (y = 2333.5x + 2956.2; r2 = 0.9979), repeatability with respect to retention time (CV = 0.45%) and area (CV = 0.30%), and selectivity, and possessed detection and quantification limits of 0.18 and 0.85 µg·mL?1, respectively. Different cashew clones containing AnAc were extracted and analyzed using the proposed method. A recovery of >90% was achieved using two sequential extractions. The total AnAc content ranged from 128.35 to 217.00 mg·100 g?1 in peduncle samples obtained from five different cashew clones. 650 $aLiquid chromatography 650 $aAnacardium Occidentale 653 $aAnacardic acid 653 $aHPLC 653 $aValidation 700 1 $aMITRI, M. P. 700 1 $aZOCOLO, G. J. 700 1 $aCANUTO, K. M. 700 1 $aBRITO, E. S. de 773 $tFoods$gv. 12, n. 2759, 2023.
Download
Esconder MarcMostrar Marc Completo |
Registro original: |
Embrapa Alimentos e Territórios (CNAT) |
|
Biblioteca |
ID |
Origem |
Tipo/Formato |
Classificação |
Cutter |
Registro |
Volume |
Status |
Fechar
|
Nenhum registro encontrado para a expressão de busca informada. |
|
|