Data/hora: 21/06/2024 10:18:12

Biblioteca(s): 	Embrapa Florestas.	
Data corrente: 	11/04/2018	
Data da última atualização: 	07/05/2018	
Autoria: 	LIMA, N. K.; LOPES, A. R.; GUERRERO JÚNIOR, P. G.; YAMAMOTO, C. I.; HANSEL, F. A.	
Afiliação: 	NATHALYA KOSINSKI LIMA, UFPR; ANDRÉ ROMUALDO LOPES, UFPR; PALIMECIO GIMENES GUERRERO JÚNIOR, UFPR; CARLOS ITSUO YAMAMOTO, UFPR; FABRICIO AUGUSTO HANSEL, CNPF.	
Título: 	Determination of volatile organic compounds in eucalyptus fast pyrolysis bio-oil by full evaporation headspace gas chromatography.	
Ano de publicação: 	2018	
Fonte/Imprenta: 	Talanta, v. 176, p. 47-51, Jan. 2018.	
DOI: 	10.1016/j.talanta.2017.08.008	
Idioma: 	Inglês	
Conteúdo: 	This paper reports a full evaporation (FE) headspace gas chromatographic (HS-GC) method for the determination of the volatile organic compounds (VOCs) in bio-oil (i.e. methanol, ethanol, acetone, acetic acid and furfural). The method uses a 4 ?L sample of bio-oil in a headspace vial (ca. 20 mL). Complete evaporation of the compounds was achieved after seven minutes at 90 °C. The method showed good precision and accuracy for methanol, ethanol, acetone and acetic acid. The recovery of furfural was low (74.3%). The results showed that the protocol can be applied for the determination of methanol, ethanol, acetone and acetic acid in bio-oil. Detection limits ranged from 0.13 to 0.16 ?g. Acetic acid was the dominant analyte in the heavy bio-oil and light bio-oil analysis (113. 3 and 85.1 ?g mg?1, respectively), followed by methanol, ethanol, and acetone. The polymerisation of furfural was suspected as the cause of its poor quantification.	
Palavras-Chave: 	FID.	
Thesagro: 	Biocombustível; Biomassa; Eucalipto; Madeira.	
Thesaurus Nal: 	Biofuels; Biomass; Eucalyptus; Wood.	
Categoria do assunto: 	X Pesquisa, Tecnologia e Engenharia	
Registro original: 	Embrapa Florestas (CNPF)	
Exemplares: 	CNPF - (56318-1) - UPC - AP - DD -  -  -  - DIS