| |
|
|
 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
|
Registro Completo |
|
Biblioteca(s): |
Embrapa Pecuária Sudeste. |
|
Data corrente: |
01/09/2017 |
|
Data da última atualização: |
13/11/2017 |
|
Tipo da produção científica: |
Artigo em Periódico Indexado |
|
Autoria: |
MACHADO, R. C.; AMARAL, C. D. B. do; NOBREGA, J. de A.; NOGUEIRA, A. R. de A. |
|
Afiliação: |
Raquel Cardoso Machado, UFSCAR; Clarice Dias Britto do Amaral, UFPR; Joaquim de Araújo Nobrega, UFSCar; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
|
Título: |
Multielemental determination of As, Bi, Ge, Sb, and Sn in agricultural samples using hydride generation coupled to microwave-induced plasma optical emission spectrometry. |
|
Ano de publicação: |
2017 |
|
Fonte/Imprenta: |
Journal of Agricultural and Food Chemistry, v. 65, n. 23, p. 4839-4842, 2017. |
|
DOI: |
10.1021/acs.jafc.7b01448 |
|
Idioma: |
Inglês |
|
Conteúdo: |
A microwave-induced plasma optical emission spectrometer with N2-based plasma was combined with a multimode sample introduction system (MSIS) for hydride generation (HG) and multielemental determination of As, Bi, Ge, Sb, and Sn in samples of forage, bovine liver, powdered milk, agricultural gypsum, rice, and mineral fertilizer, using a single condition of prereduction and reduction. The accuracy of the developed analytical method was evaluated using certified reference materials of water and mineral fertilizer, and recoveries ranged from 95 to 106%. Addition and recovery experiments were carried out, and the recoveries varied from 85 to 117% for all samples evaluated. The limits of detection for As, Bi, Ge, Sb, and Sn were 0.46, 0.09, 0.19, 0.46, and 5.2 μg/L, respectively, for liquid samples, and 0.18, 0.04, 0.08, 0.19, and 2.1 mg/kg, respectively, for solid samples. The method proposed offers a simple, fast, multielemental, and robust alternative for successful determination of all five analytes in agricultural samples with low operational cost without compromising analytical performance. |
|
Palavras-Chave: |
Microwave-induced plasm; Nitrogen plasma; Simultaneous hydride generation. |
|
Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
|
Marc: |
LEADER 01882naa a2200205 a 4500
001 2074823
005 2017-11-13
008 2017 bl uuuu u00u1 u #d
024 7 $a10.1021/acs.jafc.7b01448$2DOI
100 1 $aMACHADO, R. C.
245 $aMultielemental determination of As, Bi, Ge, Sb, and Sn in agricultural samples using hydride generation coupled to microwave-induced plasma optical emission spectrometry.$h[electronic resource]
260 $c2017
520 $aA microwave-induced plasma optical emission spectrometer with N2-based plasma was combined with a multimode sample introduction system (MSIS) for hydride generation (HG) and multielemental determination of As, Bi, Ge, Sb, and Sn in samples of forage, bovine liver, powdered milk, agricultural gypsum, rice, and mineral fertilizer, using a single condition of prereduction and reduction. The accuracy of the developed analytical method was evaluated using certified reference materials of water and mineral fertilizer, and recoveries ranged from 95 to 106%. Addition and recovery experiments were carried out, and the recoveries varied from 85 to 117% for all samples evaluated. The limits of detection for As, Bi, Ge, Sb, and Sn were 0.46, 0.09, 0.19, 0.46, and 5.2 μg/L, respectively, for liquid samples, and 0.18, 0.04, 0.08, 0.19, and 2.1 mg/kg, respectively, for solid samples. The method proposed offers a simple, fast, multielemental, and robust alternative for successful determination of all five analytes in agricultural samples with low operational cost without compromising analytical performance.
653 $aMicrowave-induced plasm
653 $aNitrogen plasma
653 $aSimultaneous hydride generation
700 1 $aAMARAL, C. D. B. do
700 1 $aNOBREGA, J. de A.
700 1 $aNOGUEIRA, A. R. de A.
773 $tJournal of Agricultural and Food Chemistry$gv. 65, n. 23, p. 4839-4842, 2017.
Download
Esconder MarcMostrar Marc Completo |
|
Registro original: |
Embrapa Pecuária Sudeste (CPPSE) |
|
|
Biblioteca |
ID |
Origem |
Tipo/Formato |
Classificação |
Cutter |
Registro |
Volume |
Status |
URL |
Voltar
|
|
|
| Registros recuperados : 5 | |
| 2. |  | LEMOS, E. C. M.; VASCONCELOS, S. S.; BARROS, J. M.; SILVA, A. K. L. Respiração do solo em sistemas de produção agropecuária no Nordeste Paraense. In: SEMINÁRIO GESTABACIAS, 1., 2010, Belém, PA. Resultados de pesquisas em mesobacias do Nordeste paraense e sua aplicação no desenvolvimento rural. Belém, PA: Embrapa Amazônia Oriental: Projeto Gestabacias, 2010. 1 CD-ROM.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Amazônia Oriental. |
|    |
| 4. | | LEMOS, E. C. M.; VASCONCELOS, S. S.; BARROS, J. M.; SILVA, A. K. L.; CARVALHO, C. J. R. de. Variação sazonal da respiração do solo em diferentes sistemas de produção agropecuária na Amazônia Oriental. In: REUNIÃO BRASILEIRA DE FERTILIDADE DO SOLO E NUTRIÇÃO DE PLANTAS, 29.; REUNIÃO BRASILEIRA SOBRE MICORRIZAS, 13.; SIMPÓSIO BRASILEIRO DE MICROBIOLOGIA DO SOLO, 11.; REUNIÃO BRASILEIRA DE BIOLOGIA DO SOLO, 8., 2010, Guarapari. Fontes de nutrientes e produção agrícola: modelando o futuro: anais. Viçosa, MG: SBCS, 2010. FERTBIO 2010.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Amazônia Oriental. |
|  |
| 5. | | LEMOS, E. C. M.; VASCONCELOS, S. S.; SANTIAGO, M. R.; OLIVEIRA JUNIOR, M. C. M. de; SOUZA, C. M. de A. The responses of soil, litter and root carbon stocks to the conversion of forest regrowth to crop and tree production systems used by smallholder farmers in eastern Amazonia. Soil Use and Management, v. 32, n. 4, p. 504-514, Dec. 2016.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 2 |
| Biblioteca(s): Embrapa Amazônia Oriental. |
| |
| Registros recuperados : 5 | |
|
| Nenhum registro encontrado para a expressão de busca informada. |
|
|
