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Registro Completo |
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Biblioteca(s): |
Embrapa Semiárido. |
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Data corrente: |
11/02/2021 |
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Data da última atualização: |
12/02/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
SILVA, C. B. da; DUARTE, D. S.; SOUZA, A. V. de; ASSIS, O. B. G. de; BRITTO, D. de. |
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Afiliação: |
Cristina Barbosa da Silva; Dirliane Santos Duarte; ANA VALERIA VIEIRA DE SOUZA, CPATSA; ODILIO BENEDITO GARRIDO DE ASSIS, CNPDIA; DOUGLAS DE BRITTO, CPATSA. |
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Título: |
Synthesis of chitosan polysaccharide nanoparticles for skin grape extract stabilization. |
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Ano de publicação: |
2020 |
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Fonte/Imprenta: |
Brazilian Journal of Development, v. 6, n. 4, p. 17913-17930, 2020. |
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Idioma: |
Inglês |
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Conteúdo: |
Nanoparticles obtained by chitosan and tripolyphosphatehas been largely studied due to its entrapment characteristics. However, several parameters can influence the synthesis and encapsulationprocesses. In this way, this work proposed to study the nanoparticle formation with chitosan and tripolyphosphate in function of the acid concentration (1.0; 0.5 and0.1%) and the kind of the acid (hydrochloric and acetic). Conductometric and Potentiometric techniques showed that the reactional system was very dependent on the pH variation. The best condition, both for HCl and acetic acid, was achieved for systems with lower pH variation. For such systems, Dynamic Light Scattering technique showed formation of nanoparticle with the lowest size (135±7 nm) and higher stability (zeta potential near 30 mV). Also, by Scanning Electronic Microscopy, such systems exhibited good morphological aspect, with nanoparticles having spherical shape and lower level of agglomeration. The cryoprotection with sucrose solution before freeze-drying was fundamental to get samples with the improved re-suspension ability and preserved nanoparticle character. By UV-visible spectrophotometry, both HCl and acetic acid-based systems resulted in nanoparticles with good polyphenols encapsulation efficiency (~70%). The release profile was pH-dependent. In this way, the chitosan and tripolyphosphate ionic gelification need an accurate pH control both in the synthesis and in the encapsulation-release processes. |
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Palavras-Chave: |
Casca de uva; Encapsulamento; Hidrogel; Nanopartículas; Polieletrólito; Polifenóis; Quitosana; Reticulação iônica. |
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Thesagro: |
Uva. |
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Thesaurus Nal: |
Grapes. |
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Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/221168/1/Synthesis-of-chitosan-polysaccharide-nanoparticle-2020.pdf
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Marc: |
LEADER 02306naa a2200289 a 4500
001 2130000
005 2021-02-12
008 2020 bl uuuu u00u1 u #d
100 1 $aSILVA, C. B. da
245 $aSynthesis of chitosan polysaccharide nanoparticles for skin grape extract stabilization.$h[electronic resource]
260 $c2020
520 $aNanoparticles obtained by chitosan and tripolyphosphatehas been largely studied due to its entrapment characteristics. However, several parameters can influence the synthesis and encapsulationprocesses. In this way, this work proposed to study the nanoparticle formation with chitosan and tripolyphosphate in function of the acid concentration (1.0; 0.5 and0.1%) and the kind of the acid (hydrochloric and acetic). Conductometric and Potentiometric techniques showed that the reactional system was very dependent on the pH variation. The best condition, both for HCl and acetic acid, was achieved for systems with lower pH variation. For such systems, Dynamic Light Scattering technique showed formation of nanoparticle with the lowest size (135±7 nm) and higher stability (zeta potential near 30 mV). Also, by Scanning Electronic Microscopy, such systems exhibited good morphological aspect, with nanoparticles having spherical shape and lower level of agglomeration. The cryoprotection with sucrose solution before freeze-drying was fundamental to get samples with the improved re-suspension ability and preserved nanoparticle character. By UV-visible spectrophotometry, both HCl and acetic acid-based systems resulted in nanoparticles with good polyphenols encapsulation efficiency (~70%). The release profile was pH-dependent. In this way, the chitosan and tripolyphosphate ionic gelification need an accurate pH control both in the synthesis and in the encapsulation-release processes.
650 $aGrapes
650 $aUva
653 $aCasca de uva
653 $aEncapsulamento
653 $aHidrogel
653 $aNanopartículas
653 $aPolieletrólito
653 $aPolifenóis
653 $aQuitosana
653 $aReticulação iônica
700 1 $aDUARTE, D. S.
700 1 $aSOUZA, A. V. de
700 1 $aASSIS, O. B. G. de
700 1 $aBRITTO, D. de
773 $tBrazilian Journal of Development$gv. 6, n. 4, p. 17913-17930, 2020.
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Registro original: |
Embrapa Semiárido (CPATSA) |
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| Registros recuperados : 115 | |
| 3. |  | SOUZA, A. V. de. Propagação in vitro de espécies da Caatinga. In: WORKSHOP DE TECNOLOGIAS E FISIOLOGIA DE SEMENTES E MUDAS DE ESPÉCIES ARBÓREAS NATIVAS DA CAATINGA, 3., 2011, Petrolina. Anais... Petrolina: Embrapa Semiárido, 2011. 1 CD-ROM.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 12. | | SOUZA, A. V. de; BERTONI, B. W.; FRANÇA, S. C.; PEREIRA, A. M. S. Conservação e enraizamento in vitro de infalível (Mandevilla velutina K. Schum.), uma planta medicinal do Cerrado. Revista Brasileira de Plantas Medicinais, Botucatu, v. 13, n. 3, p. 319-327, 2011.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: B - 2 |
| Biblioteca(s): Embrapa Semiárido. |
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| 18. | | SOUZA, A. V. de; BERTONI, B. W.; FRANÇA, S. de C.; PEREIRA, A. M. S. Micorrizas arbusculares em populações naturais de catuaba (Anemopaegma arvense (Vell.) Stell. ex de Souza). In: CONGRESSO NACIONAL DE BOTÂNICA, 60.; REUNIÃO NORDESTINA DE BOTÂNICA, 32.; ERBOT - ENCONTRO REGIONAL DE BOTÂNICOS - MG, BA , ES, 29., 2009, Feira de Santana. Botânica brasileira: futuro e compromissos. Feira de Santana: SBB: UEFS, 2009. 1 CD-ROM.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 19. | | SILVA, N. G. B.; SOUZA, A. V. de; SOUZA, D. D.; OLIVEIRA, F. J. V. Tipo de estaca e concentração de ácido indol butírico no enraizamento de alecrim da chapada. Horticultura Brasileira, v. 30, n. 2, p. S6016-S6022, jul. 2012. 1 CD-ROM. Suplemento. Edição dos Anais do 52 Congresso Brasileiro de Olericultura, Salvador, jul. 2012.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 20. | | SOUZA, A. V. de; BERTONI, B. W.; FRANÇA, S. de C.; PEREIRA, A. M. S. Enraizamento in vitro de catuaba (Anemopaegma arvense ) (Vell.) Stell. ex de Souza. In: CONGRESSO NACIONAL DE BOTÂNICA, 60.; REUNIÃO NORDESTINA DE BOTÂNICA, 32.; ERBOT - ENCONTRO REGIONAL DE BOTÂNICOS - MG, BA , ES, 29., 2009, Feira de Santana. Botânica brasileira: futuro e compromissos. Feira de Santana: SBB: UEFS, 2009. 1 CD-ROM.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| Registros recuperados : 115 | |
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