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Registro Completo |
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
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Data corrente: |
20/04/2000 |
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Data da última atualização: |
18/04/2022 |
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Tipo da produção científica: |
Resumo em Anais de Congresso |
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Autoria: |
NOGUEIRA, A. R. de A.; ARAÚJO, G. C. L.; NÓBREGA, J. A. |
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Afiliação: |
ANA RITA DE ARAUJO NOGUEIRA, CPPSE; GEÓRGIA C. L. ARAÚJO, UFSCAR; JOAQUIM A. NÓBREGA, UFSCAR. |
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Título: |
Acid vapor sample decomposition in open vessel microwave. |
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Ano de publicação: |
2000 |
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Fonte/Imprenta: |
In: PITTCON, 21., 2000, New Orleans. Abstracts... New Orleans: PITTCON, 2000. |
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Idioma: |
Português |
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Conteúdo: |
Micrawave decomposition has been increasingly used hr a large number of samples. A method using an open vessel microwave was used for biological sample preparation with nitric acid vapors under atmospheric pressure. A lab made Teflon@ support suited with four cups, which received the samples, was inserted in the microwave vessel. These cups were used to weight 30 mg of certi5ed re5wence materials such as spinach and apple leaves, which received 150 pL of d.i. water to improve the micrawave e%ciency. This mixture was exposed to acid vapor stemmed from 15 mL of concentrated nitrie acid plsced in the bottom of the vessel hr decompoeition. The maximum microwave temperature, 115'C, was reached in 4 min. This condition was rnaintained hr 20 min to sllow complete decomposition of the sample. The deeomposed sample, in the cup, was diluted to 1.0 mL of d.i. water, shaken and centrifuged. The cups were than placed directed into an autosampler for Co and Fe analysis in an atomic absorption graphite fumace spectrometer. |
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Palavras-Chave: |
Acid vapor; Decompostion; Microvawe; Open vessel. |
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Thesaurus Nal: |
cobalt. |
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Categoria do assunto: |
W Química e Física |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/118360/1/digitalizar0004.pdf
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Marc: |
LEADER 01589nam a2200193 a 4500
001 1044768
005 2022-04-18
008 2000 bl uuuu u00u1 u #d
100 1 $aNOGUEIRA, A. R. de A.
245 $aAcid vapor sample decomposition in open vessel microwave.$h[electronic resource]
260 $aIn: PITTCON, 21., 2000, New Orleans. Abstracts... New Orleans: PITTCON$c2000
520 $aMicrawave decomposition has been increasingly used hr a large number of samples. A method using an open vessel microwave was used for biological sample preparation with nitric acid vapors under atmospheric pressure. A lab made Teflon@ support suited with four cups, which received the samples, was inserted in the microwave vessel. These cups were used to weight 30 mg of certi5ed re5wence materials such as spinach and apple leaves, which received 150 pL of d.i. water to improve the micrawave e%ciency. This mixture was exposed to acid vapor stemmed from 15 mL of concentrated nitrie acid plsced in the bottom of the vessel hr decompoeition. The maximum microwave temperature, 115'C, was reached in 4 min. This condition was rnaintained hr 20 min to sllow complete decomposition of the sample. The deeomposed sample, in the cup, was diluted to 1.0 mL of d.i. water, shaken and centrifuged. The cups were than placed directed into an autosampler for Co and Fe analysis in an atomic absorption graphite fumace spectrometer.
650 $acobalt
653 $aAcid vapor
653 $aDecompostion
653 $aMicrovawe
653 $aOpen vessel
700 1 $aARAÚJO, G. C. L.
700 1 $aNÓBREGA, J. A.
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Registro original: |
Embrapa Pecuária Sudeste (CPPSE) |
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| Registros recuperados : 223 | |
| 4. |  | TREVISAN, L. C.; NOGUEIRA, A. R. de A.; NÓBREGA, J. A. Acid vapor partial digestion of biological samples in a focused microwave: multielement determination by ICP OES with axially-viewed configuration. In: RIO SYMPOSIUM ON ATOMIC SPECTROMETRY, 7., 2002, Florianópolis, SC. ICP Information Newsletter, v.28, n.1, june 2002. p.136. Tu34.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 7. | | GARCIA, E. E.; PEREIRA, C. D.; NOGUEIRA, A. R. de A.; NÓBREGA, J. A. Avaliação da correção de sinais de fundo causados pelos íons diatômicos Ar2 + e CN+ em ICP-MS com interface CRI. In: ENCONTRO NACIONAL DE QUÍMICA ANALÍTICA, 15.; CONGRESSO IBEROAMERICANO DE QUÍMICA ANALÍTICA, 3., 2009, Salvador, BA. Anais... Salvador: SBQ: UFBA, 2009.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 20. | | SILVA, F. V.; SILVA, C. S.; NÓBREGA, J. A.; NOGUEIRA, A. R. de A. Evaluation of inductively coupled plasma optical emission spectrometers with axially-and radially-viewed configurations. In: RIO SYMPOSIUM ON ATOMIC SPECTROMETRY, 7., 2002, Florianópolis, SC. ICP Information Newsletter, v.28, n.1, jun. 2002. 2 p.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| Registros recuperados : 223 | |
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| Nenhum registro encontrado para a expressão de busca informada. |
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