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Registro Completo |
Biblioteca(s): |
Embrapa Agroindústria de Alimentos. |
Data corrente: |
24/10/2006 |
Data da última atualização: |
13/03/2013 |
Tipo da produção científica: |
Comunicado Técnico/Recomendações Técnicas |
Autoria: |
STEPHAN, M. P.; NASCIMENTO, M. da G. F. do. |
Afiliação: |
MARILIA PENTEADO STEPHAN, CTAA. |
Título: |
Obtenção de padrão de identidade de peito de galinha através de eletroforese SDS-PAGE. |
Ano de publicação: |
2005 |
Fonte/Imprenta: |
Rio de Janeiro: Embrapa Agroindústria de Alimentos, 2005. |
Páginas: |
3 p. |
Série: |
(Embrapa Agroindústria de Alimentos. Comunicado Técnico, 84). |
ISSN: |
0103-5231 |
Idioma: |
Português |
Conteúdo: |
Eletroforese de proteínas; Preparação da amostra de extrato protéico de peito de galinha. |
Palavras-Chave: |
Peito de galinha; Proteínas. |
Thesagro: |
Eletroforese. |
Categoria do assunto: |
-- |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/CTAA-2009-09/8951/1/ct84-2005.pdf
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Marc: |
LEADER 00703nam a2200193 a 4500 001 1416514 005 2013-03-13 008 2005 bl uuuu u0uu1 u #d 022 $a0103-5231 100 1 $aSTEPHAN, M. P. 245 $aObtenção de padrão de identidade de peito de galinha através de eletroforese SDS-PAGE. 260 $aRio de Janeiro: Embrapa Agroindústria de Alimentos$c2005 300 $a3 p. 490 $a(Embrapa Agroindústria de Alimentos. Comunicado Técnico, 84). 520 $aEletroforese de proteínas; Preparação da amostra de extrato protéico de peito de galinha. 650 $aEletroforese 653 $aPeito de galinha 653 $aProteínas 700 1 $aNASCIMENTO, M. da G. F. do
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Registro original: |
Embrapa Agroindústria de Alimentos (CTAA) |
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Registro Completo
Biblioteca(s): |
Embrapa Pecuária Sudeste. |
Data corrente: |
22/08/2005 |
Data da última atualização: |
13/03/2023 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Autoria: |
SANTOS, M. C.; NOGUEIRA, A. R. de A.; NÓBREGA, J. A. |
Afiliação: |
MIRIAN C. SANTOS, Universidade Federal de São Carlos; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; JOAQUIM A. NÓBREGA, Universidade Federal de São Carlos. |
Título: |
Clay and refractory materials slurries in ductively coupled plasma optical emission spectrometry: effects of mechano chemical on emission intensities of analytes. |
Ano de publicação: |
2005 |
Fonte/Imprenta: |
Journal of Brazilian Chemical Society, v. 16, n. 3a, p. 372-380, june 2005. |
DOI: |
https://doi.org/10.1590/S0103-50532005000300010 |
Idioma: |
Inglês |
Conteúdo: |
The developed work investigated the application of mechanochemical synthesis for promoting reactions in the samples and for synthesizing new compounds for increment of emission intensities of analytes in clays and refractory materials slurries in inductively coupled plasma optical emission spectrometry with axial viewing. The hypothesis is that it is possible to generate more volatile compounds during the grinding step and these new compounds will increase the intensities of emission signals for slurries introduced in the plasma. The action of two chemical modifiers, LiBO2 and Na2CO3, added during the grinding step was evaluated. The clays and refractory materials mixed with the chemical modifier were ground for 2 h using a high impact ball mill with a tungsten carbide grinding container and balls. Slurries were prepared by dispersing the modified clays and refractory materials in 10% v v-1 HNO3 solution and by shaking them in an ultrasonic bath to ensure good dispersion. The compounds produced during the grinding step were characterised by X-ray diffraction and thermogravimetric analysis. Both techniques indicated the formation of new compounds in clays and refractory materials by mechanochemical synthesis. Chemical modification effects were evaluated by changes of the emission intensities of Al, Ca, Fe, K, Mg, P, Si, and Ti. Both modifiers caused increments of sensitivities for all analytes in up to 665% (Na2CO3) and 583% (LiBO2) compared to the emission signals for analytes present in slurries prepared using samples ground without adding modifiers. MenosThe developed work investigated the application of mechanochemical synthesis for promoting reactions in the samples and for synthesizing new compounds for increment of emission intensities of analytes in clays and refractory materials slurries in inductively coupled plasma optical emission spectrometry with axial viewing. The hypothesis is that it is possible to generate more volatile compounds during the grinding step and these new compounds will increase the intensities of emission signals for slurries introduced in the plasma. The action of two chemical modifiers, LiBO2 and Na2CO3, added during the grinding step was evaluated. The clays and refractory materials mixed with the chemical modifier were ground for 2 h using a high impact ball mill with a tungsten carbide grinding container and balls. Slurries were prepared by dispersing the modified clays and refractory materials in 10% v v-1 HNO3 solution and by shaking them in an ultrasonic bath to ensure good dispersion. The compounds produced during the grinding step were characterised by X-ray diffraction and thermogravimetric analysis. Both techniques indicated the formation of new compounds in clays and refractory materials by mechanochemical synthesis. Chemical modification effects were evaluated by changes of the emission intensities of Al, Ca, Fe, K, Mg, P, Si, and Ti. Both modifiers caused increments of sensitivities for all analytes in up to 665% (Na2CO3) and 583% (LiBO2) compared to the emission signals for analyt... Mostrar Tudo |
Palavras-Chave: |
ICP; Mechanochemical synthesis; OES; Refractory material; Slurry. |
Thesaurus NAL: |
clay. |
Categoria do assunto: |
W Química e Física |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/110387/1/a10v16n3a.pdf
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Marc: |
LEADER 02362naa a2200229 a 4500 001 1047197 005 2023-03-13 008 2005 bl uuuu u00u1 u #d 024 7 $ahttps://doi.org/10.1590/S0103-50532005000300010$2DOI 100 1 $aSANTOS, M. C. 245 $aClay and refractory materials slurries in ductively coupled plasma optical emission spectrometry$beffects of mechano chemical on emission intensities of analytes.$h[electronic resource] 260 $c2005 520 $aThe developed work investigated the application of mechanochemical synthesis for promoting reactions in the samples and for synthesizing new compounds for increment of emission intensities of analytes in clays and refractory materials slurries in inductively coupled plasma optical emission spectrometry with axial viewing. The hypothesis is that it is possible to generate more volatile compounds during the grinding step and these new compounds will increase the intensities of emission signals for slurries introduced in the plasma. The action of two chemical modifiers, LiBO2 and Na2CO3, added during the grinding step was evaluated. The clays and refractory materials mixed with the chemical modifier were ground for 2 h using a high impact ball mill with a tungsten carbide grinding container and balls. Slurries were prepared by dispersing the modified clays and refractory materials in 10% v v-1 HNO3 solution and by shaking them in an ultrasonic bath to ensure good dispersion. The compounds produced during the grinding step were characterised by X-ray diffraction and thermogravimetric analysis. Both techniques indicated the formation of new compounds in clays and refractory materials by mechanochemical synthesis. Chemical modification effects were evaluated by changes of the emission intensities of Al, Ca, Fe, K, Mg, P, Si, and Ti. Both modifiers caused increments of sensitivities for all analytes in up to 665% (Na2CO3) and 583% (LiBO2) compared to the emission signals for analytes present in slurries prepared using samples ground without adding modifiers. 650 $aclay 653 $aICP 653 $aMechanochemical synthesis 653 $aOES 653 $aRefractory material 653 $aSlurry 700 1 $aNOGUEIRA, A. R. de A. 700 1 $aNÓBREGA, J. A. 773 $tJournal of Brazilian Chemical Society$gv. 16, n. 3a, p. 372-380, june 2005.
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Embrapa Pecuária Sudeste (CPPSE) |
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