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Registro Completo |
Biblioteca(s): |
Embrapa Instrumentação. |
Data corrente: |
21/09/2021 |
Data da última atualização: |
10/06/2022 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Autoria: |
HUAMÁN, J. L. C.; NICOLODELLI, G.; SENESI, G. S.; MONTES, C. R.; PERRUCI, N. A. F.; BEZZON, V. D. N. |
Título: |
Characterization and distribution of mineral phases in an Amazonian humiluvic Spodosol profile by XRPD, HR-TEM, SAED and SEM-EDX. |
Ano de publicação: |
2021 |
Fonte/Imprenta: |
Environmental Earth Sciences, v. 80, 405, 2021. |
Páginas: |
1 - 11 |
ISSN: |
1866-6299 |
DOI: |
https://doi.org/10.1007/s12665-021-09697-1 |
Idioma: |
Inglês |
Conteúdo: |
The Amazonian biome has a fundamental role in the global climate change scenario and the understanding the physicochemical aspect in Amazonian soils is of great importance. The nine horizons constituting a typical Amazonian Spodosol profle were studied by diferent complementary techniques: X-ray powder difraction (XRPD), high-resolution transmission electron microscopy (HR-TEM), selected area electron difraction (SAED) and scanning electron microscopy-energy-dispersive X-ray spectrometry (SEM–EDX). The XRPD analysis revealed the presence of diferent minerals along the profle, i.e. quartz from 0 to 214 cm (horizons from A1 to Bhs) and kaolinite from 215 to 290 cm (horizons from Tr to K2). The HR-TEM images and SAED patterns revealed the presence of kaolinite in the horizon A1, which was not detected by XRPD. Application of the Rietveld refnement enabled the quantifcation of the minerals in each horizon. The SEM–EDX analyses allowed to identifying changes in the horizon surface morphology as a consequence of ongoing deformation. A signifcant decrease of particle sizes and a marked variations of their surface features with increasing depth were measured by SEM. In conclusion, the results of this work provide new insights into the relationship between chemical properties and mineral changes along the soil profle. |
Palavras-Chave: |
Amazonian Spodosol; Horizons structure; Rietveld method. |
Categoria do assunto: |
-- |
Marc: |
LEADER 02135naa a2200253 a 4500 001 2134632 005 2022-06-10 008 2021 bl uuuu u00u1 u #d 022 $a1866-6299 024 7 $ahttps://doi.org/10.1007/s12665-021-09697-1$2DOI 100 1 $aHUAMÁN, J. L. C. 245 $aCharacterization and distribution of mineral phases in an Amazonian humiluvic Spodosol profile by XRPD, HR-TEM, SAED and SEM-EDX.$h[electronic resource] 260 $c2021 300 $a1 - 11 520 $aThe Amazonian biome has a fundamental role in the global climate change scenario and the understanding the physicochemical aspect in Amazonian soils is of great importance. The nine horizons constituting a typical Amazonian Spodosol profle were studied by diferent complementary techniques: X-ray powder difraction (XRPD), high-resolution transmission electron microscopy (HR-TEM), selected area electron difraction (SAED) and scanning electron microscopy-energy-dispersive X-ray spectrometry (SEM–EDX). The XRPD analysis revealed the presence of diferent minerals along the profle, i.e. quartz from 0 to 214 cm (horizons from A1 to Bhs) and kaolinite from 215 to 290 cm (horizons from Tr to K2). The HR-TEM images and SAED patterns revealed the presence of kaolinite in the horizon A1, which was not detected by XRPD. Application of the Rietveld refnement enabled the quantifcation of the minerals in each horizon. The SEM–EDX analyses allowed to identifying changes in the horizon surface morphology as a consequence of ongoing deformation. A signifcant decrease of particle sizes and a marked variations of their surface features with increasing depth were measured by SEM. In conclusion, the results of this work provide new insights into the relationship between chemical properties and mineral changes along the soil profle. 653 $aAmazonian Spodosol 653 $aHorizons structure 653 $aRietveld method 700 1 $aNICOLODELLI, G. 700 1 $aSENESI, G. S. 700 1 $aMONTES, C. R. 700 1 $aPERRUCI, N. A. F. 700 1 $aBEZZON, V. D. N. 773 $tEnvironmental Earth Sciences$gv. 80, 405, 2021.
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Registros recuperados : 4 | |
1. | | HUAMÁN, J. L. C.; NICOLODELLI, G.; PEREIRA, D. M. B. Caracterização da matéria orgânica de solos Amazônicos por espectroscopia Raman e FT-IR In: JORNADA CIENTÍFICA - EMBRAPA SÃO CARLOS, 8., 2016, São Carlos, SP. Anais... São Carlos: Embrapa Instrumentação: Embrapa Pecuária Sudeste, 2016. p.45. Editores técnicos: Wilson Tadeu Lopes da Silva, José Manoel Marconcini, Maria Alice Martins, Lucimara Aparecida Forato, Paulino Ribeiro Villas Boas. (Embrapa Instrumentação. Documentos, 61).Tipo: Artigo em Anais de Congresso |
Biblioteca(s): Embrapa Instrumentação. |
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2. | | HUAMÁN, J. L. C.; TADINI, A. M.; SENESI, G. S.; MOUNIER, S.; MILORI, D. M. B. P.; NICOLODELLI, G. Characterization of an Amazon Soil Profile by Laser-Induced Breakdown, Raman, and Fluorescence Spectroscopies. Minerals, v. 13, 553, 2023. 9 p.Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 3 |
Biblioteca(s): Embrapa Instrumentação. |
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3. | | HUAMÁN, J. L. C.; NICOLODELLI, G.; SENESI, G. S.; MONTES, C. R.; PERRUCI, N. A. F.; BEZZON, V. D. N. Characterization and distribution of mineral phases in an Amazonian humiluvic Spodosol profile by XRPD, HR-TEM, SAED and SEM-EDX. Environmental Earth Sciences, v. 80, 405, 2021. 1 - 11Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 1 |
Biblioteca(s): Embrapa Instrumentação. |
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4. | | NICOLODELLI, G.; TADINI, A. M.; NOGUEIRA, M. S.; PORATAVIEIRA, S.; MOUNIER, S.; HUAMAN, J. L. C.; SANTOS, C. H.; MONTES, C. R.; MILORI, D. M. B. P. Fluorescence lifetime evaluation of whole soils from the Amazon rainforest. In: APPLIED OPTICS, v. 56, n. 24, p. 6936-6941, 2017.Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 1 |
Biblioteca(s): Embrapa Instrumentação. |
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Registros recuperados : 4 | |
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