Data/hora: 08/06/2024 04:10:11

Biblioteca(s): | Embrapa Instrumentação.
Data corrente: | 12/04/2021
Data da última atualização: | 10/06/2022
Autoria: | MORAIS, C. P.; NICOLODELLI, G.; FOSCHINI, M. M.; MOUNIER, S.; MILORI, D. M. B. P.
Afiliação: | MILENE CORSO MITSUYUKI, CNPDIA; DEBORA MARCONDES BASTOS PEREIRA, CNPDIA.
Título: | Optimization of laser-induced breakdown spectroscopy parameters from the design of experiments for multi-element qualitative analysis in river sediment.
Ano de publicação: | 2021
Fonte/Imprenta: | Spectrochimica Acta Part B: Atomic Spectroscopy, v. 177, 106066, 2021.
ISSN: | 0584-8547
DOI: | https://doi.org/10.1016/j.sab.2021.106066
Idioma: | Inglês
Conteúdo: | Laser-induced breakdown spectroscopy (LIBS) is a fast, low analytical cost, environmentally clean technique that does not require the use of reagents for sample preparation. However, regardless of the LIBS setup, it has limitations in terms of sensitivity and precision, especially when applied to complex samples, such as river sediment. To overcome these limitations, in this work, different experimental parameters were optimized for multi-element analysis of a river sediment sample using design of experiments (DOE) approaches, i.e., fractional factorial and central composite designs (CCD). The findings demonstrated that DOE applied to the LIBS technique can be used as an efficient tool for optimizing the key parameters affecting sediment analysis by LIBS.
Palavras-Chave: | Central composite design; Design of experiments; Fractional factorial design; LIBS.
Categoria do assunto: | --
Registro original: | Embrapa Instrumentação (CNPDIA)
Exemplares: | CNPDIA - (17756-1) - UPC - AP - DD - PROCI.21/20 -  - 2021/20 - DIS