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 | Acesso ao texto completo restrito à biblioteca da Embrapa Agroindústria de Alimentos. Para informações adicionais entre em contato com ctaa.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Agroindústria de Alimentos. |
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Data corrente: |
25/05/2016 |
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Data da última atualização: |
04/09/2025 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
ANJOS, M. R. dos; CASTRO, I. M. de; SOUZA, M. de L. M. de; LIMA, V. V. DE; AQUINO-NETO, F. R. DE. |
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Afiliação: |
MARIANNA RAMOS DOS ANJOS, CTAA; IZABELA MIRANDA DE CASTRO, CTAA; MARIA DE LOURDES MENDES DE SOUZA, CTAA; VIRGÍNIA VERÔNICA DE LIMA, UNIVERSIDADE FEDERAL DO RIO DE JANEIRO; FRANCISCO RADLER DE AQUINO-NETO, UNIVERSIDADE FEDERAL DORIO DE JANEIRO. |
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Título: |
Multiresidue method for simultaneous analysis of aflatoxin M1, avermectins, organophosphate pesticides and milbemycin in milk by ultra-performance liquid chromatography coupled to tandem mass spectrometry. |
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Ano de publicação: |
2016 |
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Fonte/Imprenta: |
Food Additives & Contaminants. Part A: Chemistry, Analysis, Control, Exposure & Risk Assessment, v. 33, n. 6, p. 995-1002, jun. 2016. |
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ISSN: |
1944-0049 |
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DOI: |
https://doi.org/10.1080/19440049.2016.1175227 |
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Idioma: |
Inglês |
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Conteúdo: |
A method developed for the simultaneous analysis of aflatoxin M1, abamectin, doramectin, eprinomectin, ivermectin, moxidectin, acephate, azinphos-ethyl, azinphos-methyl, diazinon, methamidophos, methidathion, mevinphos, pirimiphos-ethyl and pirimiphos-methyl in whole raw milk, based on the QuEChERS method for extraction and clean-up, with detection and quantification by ultra-performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS) is described. The method was validated according to parameters of the Analytical Quality Assurance Manual from the Brazilian Ministry of Agriculture and Commission Decision 2002/657/EC, and proved suitable for analysis of these analytes within the proposed working range, with recovery values between 77% and 110%, a standard deviation lower than 20%, limits of detection between 0.05 and 0.99 µg l(-)(1), and limits of quantification between 0.15 and 1.98 µg l(-1). Samples from animals treated with abamectin, doramectin, ivermectin and diazinon were analysed by the validated method. Residues of aflatoxin M1 were also found in field samples at levels below the established maximum residue limit. |
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Palavras-Chave: |
Macrocyclic lactones; Organophosphate pesticides; QuEChERS; UPLC-MS/MS. |
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Thesagro: |
Leite; Pesticida. |
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Thesaurus Nal: |
aflatoxin M1; milk. |
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Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
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Marc: |
LEADER 02214naa a2200289 a 4500
001 2045738
005 2025-09-04
008 2016 bl uuuu u00u1 u #d
022 $a1944-0049
024 7 $ahttps://doi.org/10.1080/19440049.2016.1175227$2DOI
100 1 $aANJOS, M. R. dos
245 $aMultiresidue method for simultaneous analysis of aflatoxin M1, avermectins, organophosphate pesticides and milbemycin in milk by ultra-performance liquid chromatography coupled to tandem mass spectrometry.$h[electronic resource]
260 $c2016
520 $aA method developed for the simultaneous analysis of aflatoxin M1, abamectin, doramectin, eprinomectin, ivermectin, moxidectin, acephate, azinphos-ethyl, azinphos-methyl, diazinon, methamidophos, methidathion, mevinphos, pirimiphos-ethyl and pirimiphos-methyl in whole raw milk, based on the QuEChERS method for extraction and clean-up, with detection and quantification by ultra-performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS) is described. The method was validated according to parameters of the Analytical Quality Assurance Manual from the Brazilian Ministry of Agriculture and Commission Decision 2002/657/EC, and proved suitable for analysis of these analytes within the proposed working range, with recovery values between 77% and 110%, a standard deviation lower than 20%, limits of detection between 0.05 and 0.99 µg l(-)(1), and limits of quantification between 0.15 and 1.98 µg l(-1). Samples from animals treated with abamectin, doramectin, ivermectin and diazinon were analysed by the validated method. Residues of aflatoxin M1 were also found in field samples at levels below the established maximum residue limit.
650 $aaflatoxin M1
650 $amilk
650 $aLeite
650 $aPesticida
653 $aMacrocyclic lactones
653 $aOrganophosphate pesticides
653 $aQuEChERS
653 $aUPLC-MS/MS
700 1 $aCASTRO, I. M. de
700 1 $aSOUZA, M. de L. M. de
700 1 $aLIMA, V. V. DE
700 1 $aAQUINO-NETO, F. R. DE
773 $tFood Additives & Contaminants. Part A: Chemistry, Analysis, Control, Exposure & Risk Assessment$gv. 33, n. 6, p. 995-1002, jun. 2016.
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Embrapa Agroindústria de Alimentos (CTAA) |
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