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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
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Data corrente: |
06/07/2021 |
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Data da última atualização: |
28/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
SILVA, F. L. F. da; ANDRADE NETO, D. M.; MENEZES, F. L. de; SÁ, I. P. de; MARCANO DE HIGUERA, J.; FECHINE, P. B. A; COSTA, L. S. da; NOGUEIRA, A. R. de A.; LOPES. G. S; MATOS, W. O. |
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Afiliação: |
FRANCISCO LUAN FONSECA DA SILVA, UFC; DAVINO MACHADO ANDRADE NETO, UFC; FERNANDO L. DE MENEZES, UFC; IVERO PITA DE SA, UFSCAR; JULYMAR MARCANO DE HIGUERA, UFSCAR; PIERRE BASÍLIO ALMEIDA FECHINE, UFC; LUELC SOUZA DA COSTA, UNICAMP; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; GISELE SIMONE LOPES, UFC; WLADIANA OLIVEIRA MATOS, UFC. |
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Título: |
Non-chromatographic arsenic speciation analyses in wild shrimp (Farfantepenaeus brasiliensis) using functionalized magnetic iron-nanoparticles. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Food Chemistry, v.345, 2021, 128781. |
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Páginas: |
9 p. |
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ISSN: |
0308-8146 |
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DOI: |
https://doi.org/10.1016/j.foodchem.2020.128781 |
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Idioma: |
Inglês |
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Conteúdo: |
A new iron-magnetic nanomaterial functionalized with organophosphorus compound was used as solid-phase for arsenic speciation analysis in seafood samples by ICP-MS. The procedure was optimized using chemometric tools and the variables pH 4.0, 15 min extraction time, and 20 mg of mass of material were obtained as the optimum point. The inorganic arsenic (iAs) extracted using nanoparticles presented concentrations between 20 and 100 µg kg 1 in the evaluated samples. The method was validated for accuracy using CRMs DOLT-5 and DORM-4. It was possible to reuse the same magnetic nanomaterial for 6 successive cycles, and we obtained a detection limit of 16.4 ng kg 1. The proposed method is suitable for the use of inorganic speciation of As, presenting good accuracy, precision, relatively low cost, and acquittance to green chemistry principles. |
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Palavras-Chave: |
Arsenic speciation; ICP-MS; Inorganic arsenic; Iron-nanoparticles; Magnetic nanoparticles separation. |
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Thesaurus Nal: |
Shrimp. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 01893naa a2200337 a 4500
001 2132807
005 2021-09-28
008 2021 bl uuuu u00u1 u #d
022 $a0308-8146
024 7 $ahttps://doi.org/10.1016/j.foodchem.2020.128781$2DOI
100 1 $aSILVA, F. L. F. da
245 $aNon-chromatographic arsenic speciation analyses in wild shrimp (Farfantepenaeus brasiliensis) using functionalized magnetic iron-nanoparticles.$h[electronic resource]
260 $c2021
300 $a9 p.
520 $aA new iron-magnetic nanomaterial functionalized with organophosphorus compound was used as solid-phase for arsenic speciation analysis in seafood samples by ICP-MS. The procedure was optimized using chemometric tools and the variables pH 4.0, 15 min extraction time, and 20 mg of mass of material were obtained as the optimum point. The inorganic arsenic (iAs) extracted using nanoparticles presented concentrations between 20 and 100 µg kg 1 in the evaluated samples. The method was validated for accuracy using CRMs DOLT-5 and DORM-4. It was possible to reuse the same magnetic nanomaterial for 6 successive cycles, and we obtained a detection limit of 16.4 ng kg 1. The proposed method is suitable for the use of inorganic speciation of As, presenting good accuracy, precision, relatively low cost, and acquittance to green chemistry principles.
650 $aShrimp
653 $aArsenic speciation
653 $aICP-MS
653 $aInorganic arsenic
653 $aIron-nanoparticles
653 $aMagnetic nanoparticles separation
700 1 $aANDRADE NETO, D. M.
700 1 $aMENEZES, F. L. de
700 1 $aSÁ, I. P. de
700 1 $aMARCANO DE HIGUERA, J.
700 1 $aFECHINE, P. B. A
700 1 $aCOSTA, L. S. da
700 1 $aNOGUEIRA, A. R. de A.
700 1 $aLOPES. G. S
700 1 $aMATOS, W. O
773 $tFood Chemistry$gv.345, 2021, 128781.
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Embrapa Pecuária Sudeste (CPPSE) |
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| 1. |  | DIAS, T. A. B.; HAVERROTH, M.; PIOVEZAN, U.; FREITAS, F. O.; ANTUNES, I. F.; MACIEL, M. R. A.; LIN, C. M.; FEIJÓ, C. T.; SILVA, S. M. O. da. Agrobiodiversidade indígena: feiras, guardiões e outros movimentos. In: SANTILLI, J.; BUSTAMANTE, P. G.; BARBIERI, R. L. (Ed.). Agrobiodiversidade. Brasília, DF: Embrapa, 2015. 308 p. (Coleção transição agroecológica, 2). p. 193-221.| Tipo: Capítulo em Livro Técnico-Científico |
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