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| Registros recuperados : 92 | |
| 13. |  | UHLMANN, A.; RAMOS, M. R.; ALMEIDA, R. E. M. de. Identificação das formas de vegetação nos pedoambientes relacionados aos perfis da RCC de Goiás e Tocantins. In: SANTOS, G. G.; OLIVEIRA, V. A. de; LUMBRERAS, J. F.; COELHO, M. R.; ALMEIDA, R. E. M. de; MADARI, B. E. (ed.). Guia de campo da XIV Reunião Brasileira de Classificação e Correlação de Solos: RCC de Goiás e Tocantins. Brasília, DF: Embrapa, 2023. E-book. cap. 5.| Biblioteca(s): Embrapa Pesca e Aquicultura. |
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| 14. | | CAGLIONI, E.; CURCIO, G. R.; UHLMANN, A.; BONNET, A. Estrutura e diversidade do componente arbóreo de Floresta Atlântica no parque nacional da serra do Itajaí, Santa Catarina. Floresta, Curitiba, v. 45, n. 2, p. 289-302, abr./jun. 2015.| Biblioteca(s): Embrapa Florestas; Embrapa Pesca e Aquicultura. |
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| 17. | | UHLMANN, A.; CURCIO, G. R.; GALVÃO, F.; SILVA, S. M. Relações entre a distribuição de categorias fitofisionômicas e padrões geomórficos e pedológicos em uma área de savana (cerrado) no Estado do Paraná, Brasil. Arquivos de Biologia e Tecnologia, Curitiba, v. 40, n. 1, p. 473-483, jun. 1997.| Biblioteca(s): Embrapa Florestas. |
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| 18. | | QUINTANI, I. J.; UHLMANN, A.; VOLKMANN, A.; ZIMMER, E.; STÜRMER, S. L. Análise do desenvolvimento de espécies arbóreas com potencial para a recuperação de ambientes fluviais na Bacia Hidrográfica do Rio Itajaí - Açu em neossolo flêvico. In: CONGRESSO LATINO AMERICANO DE ECOLOGIA, 3.; CONGRESSO DE ECOLOGIA DO BRASIL, 9., 2009, São Lourenço. Ecologia e o futuro da biosfera. Anais. São Paulo: SEB, 2009. Disponível também on-line.| Biblioteca(s): Embrapa Amapá. |
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| 19. | | CAGLIONI, E.; UHLMANN, A.; CURCIO, G. R.; RAMOS, M. R.; BONNET, A.; JUNCKES, A. R. Altitude e solos determinam variações abruptas da vegetação em gradiente altitudinal de Mata Atlântica. Rodriguésia, v. 69, n. 4, p. 2055-2068, out./dez. 2018.| Biblioteca(s): Embrapa Florestas. |
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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
Registro Completo
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
|
Data corrente: |
07/07/2021 |
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Data da última atualização: |
28/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 2 |
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Autoria: |
SILVA, A. B. S. do; SÁ, I. P. de; MARCANO DE HIGUERA, J.; NOGUEIRA, A. R. de A. |
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Afiliação: |
ANA BEATRIZ SANTOS DA SILVA, UFSCAR; ÍVERO PITA DE SÁ, UFSCAR; JULYMAR MARCANO DE HIGUERA, UFSCAR; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
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Título: |
Feasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Food Analytical Methods, v.14, 2021. |
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Páginas: |
p.496-502. |
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ISSN: |
1936-976X |
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DOI: |
https://doi.org/10.1007/s12161-020-01898-x |
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Idioma: |
Inglês |
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Conteúdo: |
The dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity. |
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Palavras-Chave: |
DLLME; MIP OES; Sample preparation; Trace analysis. |
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Thesaurus NAL: |
Microextraction. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 02099naa a2200253 a 4500
001 2132839
005 2021-09-28
008 2021 bl uuuu u00u1 u #d
022 $a1936-976X
024 7 $ahttps://doi.org/10.1007/s12161-020-01898-x$2DOI
100 1 $aSILVA, A. B. S. do
245 $aFeasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES.$h[electronic resource]
260 $c2021
300 $ap.496-502.
520 $aThe dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity.
650 $aMicroextraction
653 $aDLLME
653 $aMIP OES
653 $aSample preparation
653 $aTrace analysis
700 1 $aSÁ, I. P. de
700 1 $aMARCANO DE HIGUERA, J.
700 1 $aNOGUEIRA, A. R. de A.
773 $tFood Analytical Methods$gv.14, 2021.
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