| |
|
|
| Registros recuperados : 60 | |
| 41. |  | HASHIMOTO, J. C.; PASCHOAL, J. A. R.; QUEIROZ, S. C. do N. de; FERRACINI, V. L.; ASSALIN, M. R.; REYES, F. G. R. Determinação de resíduos de verde de malaquita e verde de leucomalaquita em carne de tilápia por LC-ESI-MS/MS com extração QuEChERS. In: ENCONTRO NACIONAL, 17., E CONGRESSO LATINO AMERICANO DE ANALISTAS DE ALIMENTOS - ENAAL 2011, 3., 2011, Cuiabá.| Biblioteca(s): Embrapa Meio Ambiente. |
|    |
| 42. | | QUEIROZ, S. C. do N. de; ASSALIN, M. R.; NOBRE, S.; MELO, I. S. de; MORAES, R. M.; FERRACINI, V. L.; CERDEIRA, A. L. Determination of combretastatin A-4 in Combretun leprosum. Planta Medica, v. 76, p. 530, 2010. 9th Annual Oxford International Conference on the Science of Botanicals (ICSB), 12-15 April, 2010, University of Mississippi, USA. Poster 53.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 44. | | NUNES, K. S. D.; VALLIM, J. H.; ASSALIN, M. R.; QUEIROZ, S. C. do N. de; PARAIBA, L. C.; JONSSON, C. M.; REYES, F. G. R. Depletion study, withdrawal period calculation and bioaccumulation of sulfamethazine in tilapia (Oreochromis niloticus) treated with medicated feed. Chemosphere, v. 197, p. 89-85, 2018.| Biblioteca(s): Embrapa Meio Ambiente. |
|  |
| 45. | | FAY, E. F.; CASTRO, V. L. S. S. de; SILVA, C. M. M. de S.; ABAKERLI, R. B.; ASSALIN, M. R.; EBERLIN, M. N. Metabolização do herbicida sulfentrazona: obtenção e identificação de 3-idroximetilsulfentrazona em urina de mamíferos. In: CONGRESO VIRTUAL IBEROAMERICANO SOBRE GESTIÓN DE CALIDAD EN LABORATORIOS, 4., 2007, Barcelona. Resúmenes... Barcelona: Ministerio de Agricultura, Pesca Y Alimentación, 2007. 2 p.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 47. | | MASCARIN, G. M.; MARINHO-PRADO, J. S.; ASSALIN, M. R.; MARTINS, L. G.; BRAGA, E. S.; TASIC, L.; DITA RODRIGUES, M. A.; LOPES, R. B. Natural occurrence of Beauveria caledonica, pathogenicity to Cosmopolites sordidus and antifungal activity against Fusarium oxysporum f. sp. cubense. Pest Management Science, v. 78, n. 11, p. 4458-4470, 2022.| Biblioteca(s): Embrapa Meio Ambiente; Embrapa Recursos Genéticos e Biotecnologia. |
| |
| 48. | | CLEMENTE, Z.; JONSSON, C. M.; PRESTES, E. B.; FERRACINI, V. L.; QUEIROZ, S. C. do N. de; ASSALIN, M. R.; SILVA, S. R. C. M. Toxicidade aguda de efluentes de lavagem de equipamentos agrícolas após tratamento por fotocatálise heterogênea solar. In: CONGRESSO BRASILEIRO DE TOXICOLOGIA, 17., 2011, Ribeirão Preto. Anais... Ribeirão Preto: Sociedade Brasileira de Toxicologia, 2011. Poster AM25.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 49. | | ASSALIN, M. R.; SOUZA, D. R. C. de; ROSA, M. A.; MOLTOCARO, R. C. R.; CASTANHA, R. F.; VILELA, E. S. D.; TASIC, L.; DURÁN, N. Thiamethoxam used as nanopesticide for the effective management of Diaphorina citri psyllid: an environmental-friendly formulation. International Journal of Pest Management, p.1-9, 2022. Online first.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 50. | | BARIZON, R. R. M.; KUMMROW, F.; ALBUQUERQUE, A. F.; ASSALIN, M. R.; ROSA, M. A.; SOUZA, D. R. C. de; PAZIANOTTO, R. A. A. Surface water contamination from pesticide mixtures and risks to aquatic life in a high-input agricultural region of Brazil. Chemosphere, v. 308, pt. 3, article 136400, 2022. p. 1-10.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 51. | | HASHIMOTO, J. C.; PASCHOAL, J. A. R.; QUEIROZ, S. C. do N. de; FERRACINI, V. L.; ASSALIN, M. R.; REYES, F. G. R. A simple method for the determination of malachite green and leucomalachite green residues in fish by a modified QuEChERS extraction and LC/MS/MS. Journal of AOAC International, Arlington, v. 95, n. 3, p. 913-922, 2012.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 52. | | NUNES, K. S. D.; VALLIM, J. H.; ASSALIN, M. R.; QUEIROZ, S. C. do N. de; PARAIBA, L. C.; JONSSON, C. M.; REYES, F. G. R. Residue depletion study, withdrawal period calculation and bioaccumulation of sulfamethazine in tilapia (Oreochromis niloticus) treated with medicated feed. Journal of Veterinary Pharmacology and Therapeutics, v. 41, n. 1, june 2018. Special Issue of the abstracts 14th International Congress of the European Association for Veterinary Pharmacology and Toxicology, June 24-27 June 2018, held a Wroclaw, Poland. Ref. P9.13. p. 123.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 53. | | SOUZA, D. R. C. de; ASSALIN, M. R.; QUEIROZ, S. C. do N. de; FERRACINI, V. L.; ROSA, M. A.; TAVARES, M. M.; FERREIRA, G. T. Validação de metodologia para análise de alguns herbicidas em água de rio por LC-ESI-MS/MS. In: CONGRESSO LATINO-AMERICANO DE CROMATOGRAFIA E TÉCNICAS RELACIONADAS, 12., 2008, Florianóplis. Livro de resumos... Florianóplis: Instituto Internacional de Cromatografia, 2008. 1 CD-ROM| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 54. | | VALLIM, J. H.; CLEMENTE, Z.; CASTANHA, R. F.; PEREIRA, A. do E. S.; CAMPOS, E. V. R.; ASSALIN, M. R.; MAURER-MORELLI, C. V.; FRACETO, L. F.; CASTRO, V. L. S. S. de. Chitosan nanoparticles containing the insecticide dimethoate: a new approach in the reduction of harmful ecotoxicological effects. NanoImpact, v. 27, article 100408, 2022.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 55. | | BAPTISTA, R. C.; FERNANDES, M. A. M.; GILAVERTE, S.; QUEIROZ, S. C. do N. de; FERRACINI, V. L.; ASSALIN, M. R.; MONTEIRO, A. L. G.; REYES, F. G. R. Pharmacokinetic parameters of moxidectin residue in the serum of lambs. In: ANNUAL MEETING BRAZILIAN SOCIETY OF ANIMAL SCIENCE, 50., 2013, Campinas. The integration of knowledge in animal production: abstracts. Campinas: SBZ, 2013. 1 CD ROM.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 56. | | BAPTISTA, R. C.; FERNANDES, M. A. M.; GILAVERTE, S.; QUEIROZ, S. C. do N. de; ASSALIN, M. R.; FERRACINI, V. L.; MONTEIRO, A. L. G.; REYES, F. G. R. Determination of moxidectin in serum by liquid chromatography-tandem mass spectrometry and its application in pharmacokinetic study in lambs. Journal of the Brazilian Chemical Society, Campinas, v. 28, n. 2, p. 250-256, 2017.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 57. | | MONTEIRO, R. T. R.; SILVA, G. H. da; MESSIAS, T. G.; QUEIROZ, S. C. do N. de; ASSALIN, M. R.; SOUZA, D. R. C. de; ALVES, C. H. R.; FERREIRA, A. C.; BLAISE, C. Chemical and ecotoxicological assessments of water samples before and after being processed by a water treatment plant. Revista Ambiente & Água, Taubaté, v. 9, n. 1, p. 6-18, 2014.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 58. | | ASSALIN, M. R.; SANTOS, L. D. L. dos; SOUZA, D. R. C. de; ROSA, M. A.; MOLTOCARO, R. C. R.; CASTANHA, R. F.; DONAIRE, P. P. R.; DURAN, N. Ecotoxicity evaluation: preparation of poly-e-caprolactone and chitosannanoparticles as carriers of thiamethoxam pesticide. Journal of Physics: Conference Series, v. 1323, n. 1, 2019. Edition of the Proceedings of VI NanoSAFE International Conference, Grenoble, Nov. 2018. Article 012017.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| 59. | | PARAIBA, L. C.; FERREIRA, J. M. S.; FERRACINI, V. L.; RAMOS, S. R. R.; CERDEIRA, A. L.; ASSALIN, M. R.; PAZIANOTTO, R. A. A.; SANTOS, A. J. dos; PARAÍBA, C. C. M. Modeling pesticide translocation injected by endotherapy into the stem of coconut tree (Cocos nucifera L.). Spanish Journal of Agricultural Research, v. 20, n. 2, e1002, 2022.| Biblioteca(s): Embrapa Alimentos e Territórios; Embrapa Meio Ambiente. |
| |
| 60. | | ASSALIN, M. R.; SANTOS, L. D. L. dos; SOUZA, D. R. C. de; ROSA, M. A.; DUARTE, R. C. R. M.; CASTANHA, R. F.; DONAIRE, P. P. R.; DURAN, N. Nanoformulation as a tool for improvement of thiamethoxam encapsulation and evaluation of ecotoxicological impacts. Energy, Ecology and Environment, v. 4, n. 6. p. 310-317, 2019.| Biblioteca(s): Embrapa Meio Ambiente. |
| |
| Registros recuperados : 60 | |
|
|
|
 | Acesso ao texto completo restrito à biblioteca da Embrapa Meio Ambiente. Para informações adicionais entre em contato com cnpma.biblioteca@embrapa.br. |
Registro Completo
|
Biblioteca(s): |
Embrapa Meio Ambiente. |
|
Data corrente: |
26/07/2018 |
|
Data da última atualização: |
26/07/2018 |
|
Tipo da produção científica: |
Artigo em Periódico Indexado |
|
Circulação/Nível: |
A - 1 |
|
Autoria: |
NUNES, K. S. D.; VALLIM, J. H.; ASSALIN, M. R.; QUEIROZ, S. C. do N. de; PARAIBA, L. C.; JONSSON, C. M.; REYES, F. G. R. |
|
Afiliação: |
KATIA SANTOS DAMACENA NUNES, FEA-Unicamp; JOSE HENRIQUE VALLIM, CNPMA; MARCIA REGINA ASSALIN, CNPMA; SONIA CLAUDIA DO N DE QUEIROZ, CNPMA; LOURIVAL COSTA PARAIBA, CNPMA; CLAUDIO MARTIN JONSSON, CNPMA; FELIX GUILLERMO REYSE REYES, FEA-Unicamp. |
|
Título: |
Depletion study, withdrawal period calculation and bioaccumulation of sulfamethazine in tilapia (Oreochromis niloticus) treated with medicated feed. |
|
Ano de publicação: |
2018 |
|
Fonte/Imprenta: |
Chemosphere, v. 197, p. 89-85, 2018. |
|
Idioma: |
Inglês |
|
Conteúdo: |
Abstract: The residue depletion of sulfamethazine (SMZ) was evaluated in tilapia (Oreochromis niloticus) after 11 days of administration of medicated feed containing SMZ, at the dose of 422/mg/kg body weight (bw). The determination of SMZ in feed and tilapia fillet was carried out using the QuEChERS approach for sample preparation, and high performance liquid chromatography with diode array detector (HPLC-DAD) and ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry (UPLC-QToF-MS) for quantitation, respectively. Both methods were validated based on international and Brazilian guidelines and shown to be suitable for the intended purposes. The withdrawal period to reach the maximum residue level (MRL) of 100microgr5am/kg, according to the European Union (EU) legislative framework to all substances belonging to the sulfonamide (SA) group (EU, 2010), was 10 days (260°C-day). After treatment, the maximum level of SMZ accumulation in the tilapia muscle was 1.6?mg/kg. SMZ was shown to be quickly excreted by tilapia. Thus, considering the acceptable daily intake of SMZ established by the Codex Commission (0?0.05 mg/kg bw), and a factor of 5 times the upper amount of fish consumption in Brazil (38/kg/year), this study showed that there is a low risk of adverse effects to consumers. This study offers subsidies not only for the establishment of public policies with regard to the use of veterinary drugs currently not allowed in a country by their legal legislative framework for fish farming, but also to fish producers for the proper handling to ensure safe fish fillets. MenosAbstract: The residue depletion of sulfamethazine (SMZ) was evaluated in tilapia (Oreochromis niloticus) after 11 days of administration of medicated feed containing SMZ, at the dose of 422/mg/kg body weight (bw). The determination of SMZ in feed and tilapia fillet was carried out using the QuEChERS approach for sample preparation, and high performance liquid chromatography with diode array detector (HPLC-DAD) and ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry (UPLC-QToF-MS) for quantitation, respectively. Both methods were validated based on international and Brazilian guidelines and shown to be suitable for the intended purposes. The withdrawal period to reach the maximum residue level (MRL) of 100microgr5am/kg, according to the European Union (EU) legislative framework to all substances belonging to the sulfonamide (SA) group (EU, 2010), was 10 days (260°C-day). After treatment, the maximum level of SMZ accumulation in the tilapia muscle was 1.6?mg/kg. SMZ was shown to be quickly excreted by tilapia. Thus, considering the acceptable daily intake of SMZ established by the Codex Commission (0?0.05 mg/kg bw), and a factor of 5 times the upper amount of fish consumption in Brazil (38/kg/year), this study showed that there is a low risk of adverse effects to consumers. This study offers subsidies not only for the establishment of public policies with regard to the use of veterinary drugs currently not allowed in a country by their lega... Mostrar Tudo |
|
Palavras-Chave: |
Depletion study; LC-MS/MS; QuEChERS; Sulfadimidine; Sulfamethazine. |
|
Thesagro: |
Análise Química; Cromatografia; Espectrometria; Medicamento; Resíduo Quimico; Tilápia; Tilápia nilótica. |
|
Thesaurus NAL: |
Analytical chemistry; Analytical methods; Drug residues; Freshwater fish; High performance liquid chromatography; Ultra-performance liquid chromatography. |
|
Categoria do assunto: |
W Química e Física |
|
Marc: |
LEADER 02853naa a2200409 a 4500
001 2093569
005 2018-07-26
008 2018 bl uuuu u00u1 u #d
100 1 $aNUNES, K. S. D.
245 $aDepletion study, withdrawal period calculation and bioaccumulation of sulfamethazine in tilapia (Oreochromis niloticus) treated with medicated feed.$h[electronic resource]
260 $c2018
520 $aAbstract: The residue depletion of sulfamethazine (SMZ) was evaluated in tilapia (Oreochromis niloticus) after 11 days of administration of medicated feed containing SMZ, at the dose of 422/mg/kg body weight (bw). The determination of SMZ in feed and tilapia fillet was carried out using the QuEChERS approach for sample preparation, and high performance liquid chromatography with diode array detector (HPLC-DAD) and ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry (UPLC-QToF-MS) for quantitation, respectively. Both methods were validated based on international and Brazilian guidelines and shown to be suitable for the intended purposes. The withdrawal period to reach the maximum residue level (MRL) of 100microgr5am/kg, according to the European Union (EU) legislative framework to all substances belonging to the sulfonamide (SA) group (EU, 2010), was 10 days (260°C-day). After treatment, the maximum level of SMZ accumulation in the tilapia muscle was 1.6?mg/kg. SMZ was shown to be quickly excreted by tilapia. Thus, considering the acceptable daily intake of SMZ established by the Codex Commission (0?0.05 mg/kg bw), and a factor of 5 times the upper amount of fish consumption in Brazil (38/kg/year), this study showed that there is a low risk of adverse effects to consumers. This study offers subsidies not only for the establishment of public policies with regard to the use of veterinary drugs currently not allowed in a country by their legal legislative framework for fish farming, but also to fish producers for the proper handling to ensure safe fish fillets.
650 $aAnalytical chemistry
650 $aAnalytical methods
650 $aDrug residues
650 $aFreshwater fish
650 $aHigh performance liquid chromatography
650 $aUltra-performance liquid chromatography
650 $aAnálise Química
650 $aCromatografia
650 $aEspectrometria
650 $aMedicamento
650 $aResíduo Quimico
650 $aTilápia
650 $aTilápia nilótica
653 $aDepletion study
653 $aLC-MS/MS
653 $aQuEChERS
653 $aSulfadimidine
653 $aSulfamethazine
700 1 $aVALLIM, J. H.
700 1 $aASSALIN, M. R.
700 1 $aQUEIROZ, S. C. do N. de
700 1 $aPARAIBA, L. C.
700 1 $aJONSSON, C. M.
700 1 $aREYES, F. G. R.
773 $tChemosphere$gv. 197, p. 89-85, 2018.
Download
Esconder MarcMostrar Marc Completo |
|
Registro original: |
Embrapa Meio Ambiente (CNPMA) |
|
|
Biblioteca |
ID |
Origem |
Tipo/Formato |
Classificação |
Cutter |
Registro |
Volume |
Status |
Fechar
|
| Nenhum registro encontrado para a expressão de busca informada. |
|
|
