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 | Acesso ao texto completo restrito à biblioteca da Embrapa Suínos e Aves. Para informações adicionais entre em contato com cnpsa.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Suínos e Aves. |
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Data corrente: |
28/09/2018 |
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Data da última atualização: |
28/09/2018 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
GRESSLER, V.; FEDDERN, V.; PEIXOTO, J. de O.; LEDUR, M. C.; DALLA COSTA, O. A.; LIMA, G. J. M. M. de. |
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Afiliação: |
VANESSA GRESSLER, CNPSA; VIVIAN FEDDERN, CNPSA; JANE DE OLIVEIRA PEIXOTO, CNPSA; MONICA CORREA LEDUR, CNPSA; OSMAR ANTONIO DALLA COSTA, CNPSA; GUSTAVO JULIO MELLO M DE LIMA, CNPSA. |
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Título: |
Application of enzyme digestion and deconjugation followed by quick, easy, cheap, effective, rugged, safe extraction and liquid chromatography?tandem mass spectrometry methodology to determine ractopamine residue in pork. |
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Ano de publicação: |
2018 |
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Fonte/Imprenta: |
Journal of Food Protection, v. 81, n.8, p. 1258-1263, 2018. |
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DOI: |
10.4315/0362-028X.JFP-17-526 |
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Idioma: |
Inglês |
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Conteúdo: |
A new methodology is proposed for ractopamine residue analysis in pork. It consists of enzyme-mediated digestion and deconjugation steps; modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) extraction; and liquid chromatography?tandem mass spectrometry (LC-MS/MS). In brief, the samples were digested with protease and then deconjugated with b-glucuronidase enzyme; they were then subjected to extraction and cleanup by QuEChERS and underwent sequential analysis by LC-MS/MS. The method performance was evaluated in accordance to the validation guidelines regulated by the Brazilian Ministry of Agriculture and Food Supply. The limit of detection was 0.15 lg/kg and limit of quantification was 0.5 lg/kg. When the method was applied to real samples, ractopamine residue was found in concentrations (up to 7.86 lg/kg) below international recommendation limits up to 10 lg/kg. The method is sensitive, accurate, quick, simple, and suitable for routine analysis; therefore, it is a monitoring tool that may be adopted by laboratories to achieve compliance levels. |
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Palavras-Chave: |
B-agonista; Carne suína; Method validation; Método de validação; Músculo suíno; Ractopamina; Swine muscle. |
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Thesagro: |
Carcaça; Cromatografia; Digestão; Espectrometria; Hidrolise; Nutrição Animal; Suíno. |
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Thesaurus Nal: |
Animal nutrition; Digestion; Hydrolysis; Liquid chromatography; Mass spectrometry; Methodology; Ractopamine; Swine. |
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Categoria do assunto: |
-- |
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Marc: |
LEADER 02464naa a2200457 a 4500
001 2096560
005 2018-09-28
008 2018 bl uuuu u00u1 u #d
024 7 $a10.4315/0362-028X.JFP-17-526$2DOI
100 1 $aGRESSLER, V.
245 $aApplication of enzyme digestion and deconjugation followed by quick, easy, cheap, effective, rugged, safe extraction and liquid chromatography?tandem mass spectrometry methodology to determine ractopamine residue in pork.$h[electronic resource]
260 $c2018
520 $aA new methodology is proposed for ractopamine residue analysis in pork. It consists of enzyme-mediated digestion and deconjugation steps; modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) extraction; and liquid chromatography?tandem mass spectrometry (LC-MS/MS). In brief, the samples were digested with protease and then deconjugated with b-glucuronidase enzyme; they were then subjected to extraction and cleanup by QuEChERS and underwent sequential analysis by LC-MS/MS. The method performance was evaluated in accordance to the validation guidelines regulated by the Brazilian Ministry of Agriculture and Food Supply. The limit of detection was 0.15 lg/kg and limit of quantification was 0.5 lg/kg. When the method was applied to real samples, ractopamine residue was found in concentrations (up to 7.86 lg/kg) below international recommendation limits up to 10 lg/kg. The method is sensitive, accurate, quick, simple, and suitable for routine analysis; therefore, it is a monitoring tool that may be adopted by laboratories to achieve compliance levels.
650 $aAnimal nutrition
650 $aDigestion
650 $aHydrolysis
650 $aLiquid chromatography
650 $aMass spectrometry
650 $aMethodology
650 $aRactopamine
650 $aSwine
650 $aCarcaça
650 $aCromatografia
650 $aDigestão
650 $aEspectrometria
650 $aHidrolise
650 $aNutrição Animal
650 $aSuíno
653 $aB-agonista
653 $aCarne suína
653 $aMethod validation
653 $aMétodo de validação
653 $aMúsculo suíno
653 $aRactopamina
653 $aSwine muscle
700 1 $aFEDDERN, V.
700 1 $aPEIXOTO, J. de O.
700 1 $aLEDUR, M. C.
700 1 $aDALLA COSTA, O. A.
700 1 $aLIMA, G. J. M. M. de
773 $tJournal of Food Protection$gv. 81, n.8, p. 1258-1263, 2018.
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Registro original: |
Embrapa Suínos e Aves (CNPSA) |
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Registro Completo
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Biblioteca(s): |
Embrapa Caprinos e Ovinos; Embrapa Meio-Norte. |
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Data corrente: |
17/10/2023 |
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Data da última atualização: |
14/02/2024 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 1 |
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Autoria: |
SOUZA, H. A. de; GUEDES, F. L.; POMPEU, R. C. F. F.; ODA-SOUZA, M.; CLARK, M. V. G.; ANDRADE, H. A. F de; PRIMO, A. A.; SAGRILO, E. |
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Afiliação: |
HENRIQUE ANTUNES DE SOUZA, CPAMN; FERNANDO LISBOA GUEDES, CNPC; ROBERTO CLAUDIO FERNANDES F POMPEU, CNPC; MELISSA ODA-SOUZA, UNIVERSIDADE ESTADUAL DO PIAUÍ; MARCUS VINICIUS GUIMARAES CLARK, UNJIVERSIDADE FEDERAL DO PIAUÍ; HOSANA AGUIAR FREITAS DE ANDRADE, UNIVERSIDADE FEDERAL DO PIAUÍ; ANACLAUDIA ALVES PRIMO, UNIVERSIDADE FEDERAL DO CEARÁ; EDVALDO SAGRILO, CPAMN. |
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Título: |
Combination of organic amendments as a soil recovering strategy at a desertification hotspot in the Brazilian semiarid. |
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Ano de publicação: |
2024 |
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Fonte/Imprenta: |
Land Degradation and Development, v. 35, n. 1, p. 534-548, Jan. 2024. |
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ISSN: |
1099-145X |
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DOI: |
10.1002/ldr.4935 |
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Idioma: |
Inglês |
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Conteúdo: |
The use of manure, organic mulch, and legume-based fertilizers can increase soil fertility in semiarid regions. However, the effects of such practices on soils prone to desertification are unknown. This study aimed to evaluate soil fertility and herbaceous stratum yield on soils amended with different organic inputs in the desertification hotspot of Irauçuba, Ceará state, Brazil. The experiments were performed in two areas with different soils (Planosol and Cambisol), in randomized blocks with a 2 x 2 x 3 + 1 factorial design. The factors consisted of (i) mulch (presence or absence of Copernicia prunifera [carnauba palm] straw), (ii) manure (sheep or cattle), and (iii) legume-based fertilizer (Mimosa tenuiflora [jurema], Mimosa caesalpiniifolia [sabiá], and Leucaena leucocephala [leucena]), in addition to an untreated control, with three replicates. Soil chemical attributes and herbaceous stratum yield were assessed in the two areas. Positive effects of the combined use of carnauba palm straw, manures, and legume-based fertilizers on soil fertility were more evident for Planosol than for Cambisol. The combination of sheep manure with sabiá-based fertilizer in Planosol, and cattle manure and leucena-based fertilizer in Cambisol increased herbaceous stratum yield. Herbaceous stratum yield in Planosol is more responsive to the input of great amounts of soil nutrients (especially P) and it increases soil organic matter levels, while in Cambisol, herbaceous stratum yield is more associated with the ability of inputs to make nutrients readily available. The use of organic amendments can reverse, in the short-term, degradation and desertification processes of soils in the Brazilian semiarid region. MenosThe use of manure, organic mulch, and legume-based fertilizers can increase soil fertility in semiarid regions. However, the effects of such practices on soils prone to desertification are unknown. This study aimed to evaluate soil fertility and herbaceous stratum yield on soils amended with different organic inputs in the desertification hotspot of Irauçuba, Ceará state, Brazil. The experiments were performed in two areas with different soils (Planosol and Cambisol), in randomized blocks with a 2 x 2 x 3 + 1 factorial design. The factors consisted of (i) mulch (presence or absence of Copernicia prunifera [carnauba palm] straw), (ii) manure (sheep or cattle), and (iii) legume-based fertilizer (Mimosa tenuiflora [jurema], Mimosa caesalpiniifolia [sabiá], and Leucaena leucocephala [leucena]), in addition to an untreated control, with three replicates. Soil chemical attributes and herbaceous stratum yield were assessed in the two areas. Positive effects of the combined use of carnauba palm straw, manures, and legume-based fertilizers on soil fertility were more evident for Planosol than for Cambisol. The combination of sheep manure with sabiá-based fertilizer in Planosol, and cattle manure and leucena-based fertilizer in Cambisol increased herbaceous stratum yield. Herbaceous stratum yield in Planosol is more responsive to the input of great amounts of soil nutrients (especially P) and it increases soil organic matter levels, while in Cambisol, herbaceous stratum yield is more ... Mostrar Tudo |
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Thesagro: |
Fertilidade do Solo; Manejo do Solo. |
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Thesaurus NAL: |
Copernicia; Leucaena leucocephala subsp. leucocephala; Mimosa caesalpiniifolia; Mimosa tenuiflora; Soil fertility; Soil management. |
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Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
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Marc: |
LEADER 02735naa a2200325 a 4500
001 2157300
005 2024-02-14
008 2024 bl uuuu u00u1 u #d
022 $a1099-145X
024 7 $a10.1002/ldr.4935$2DOI
100 1 $aSOUZA, H. A. de
245 $aCombination of organic amendments as a soil recovering strategy at a desertification hotspot in the Brazilian semiarid.$h[electronic resource]
260 $c2024
520 $aThe use of manure, organic mulch, and legume-based fertilizers can increase soil fertility in semiarid regions. However, the effects of such practices on soils prone to desertification are unknown. This study aimed to evaluate soil fertility and herbaceous stratum yield on soils amended with different organic inputs in the desertification hotspot of Irauçuba, Ceará state, Brazil. The experiments were performed in two areas with different soils (Planosol and Cambisol), in randomized blocks with a 2 x 2 x 3 + 1 factorial design. The factors consisted of (i) mulch (presence or absence of Copernicia prunifera [carnauba palm] straw), (ii) manure (sheep or cattle), and (iii) legume-based fertilizer (Mimosa tenuiflora [jurema], Mimosa caesalpiniifolia [sabiá], and Leucaena leucocephala [leucena]), in addition to an untreated control, with three replicates. Soil chemical attributes and herbaceous stratum yield were assessed in the two areas. Positive effects of the combined use of carnauba palm straw, manures, and legume-based fertilizers on soil fertility were more evident for Planosol than for Cambisol. The combination of sheep manure with sabiá-based fertilizer in Planosol, and cattle manure and leucena-based fertilizer in Cambisol increased herbaceous stratum yield. Herbaceous stratum yield in Planosol is more responsive to the input of great amounts of soil nutrients (especially P) and it increases soil organic matter levels, while in Cambisol, herbaceous stratum yield is more associated with the ability of inputs to make nutrients readily available. The use of organic amendments can reverse, in the short-term, degradation and desertification processes of soils in the Brazilian semiarid region.
650 $aCopernicia
650 $aLeucaena leucocephala subsp. leucocephala
650 $aMimosa caesalpiniifolia
650 $aMimosa tenuiflora
650 $aSoil fertility
650 $aSoil management
650 $aFertilidade do Solo
650 $aManejo do Solo
700 1 $aGUEDES, F. L.
700 1 $aPOMPEU, R. C. F. F.
700 1 $aODA-SOUZA, M.
700 1 $aCLARK, M. V. G.
700 1 $aANDRADE, H. A. F de
700 1 $aPRIMO, A. A.
700 1 $aSAGRILO, E.
773 $tLand Degradation and Development$gv. 35, n. 1, p. 534-548, Jan. 2024.
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