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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
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Data corrente: |
07/07/2021 |
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Data da última atualização: |
28/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
SILVA, A. B. S. do; SÁ, I. P. de; MARCANO DE HIGUERA, J.; NOGUEIRA, A. R. de A. |
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Afiliação: |
ANA BEATRIZ SANTOS DA SILVA, UFSCAR; ÍVERO PITA DE SÁ, UFSCAR; JULYMAR MARCANO DE HIGUERA, UFSCAR; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
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Título: |
Feasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Food Analytical Methods, v.14, 2021. |
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Páginas: |
p.496-502. |
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ISSN: |
1936-976X |
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DOI: |
https://doi.org/10.1007/s12161-020-01898-x |
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Idioma: |
Inglês |
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Conteúdo: |
The dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity. |
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Palavras-Chave: |
DLLME; MIP OES; Sample preparation; Trace analysis. |
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Thesaurus Nal: |
Microextraction. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 02099naa a2200253 a 4500
001 2132839
005 2021-09-28
008 2021 bl uuuu u00u1 u #d
022 $a1936-976X
024 7 $ahttps://doi.org/10.1007/s12161-020-01898-x$2DOI
100 1 $aSILVA, A. B. S. do
245 $aFeasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES.$h[electronic resource]
260 $c2021
300 $ap.496-502.
520 $aThe dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity.
650 $aMicroextraction
653 $aDLLME
653 $aMIP OES
653 $aSample preparation
653 $aTrace analysis
700 1 $aSÁ, I. P. de
700 1 $aMARCANO DE HIGUERA, J.
700 1 $aNOGUEIRA, A. R. de A.
773 $tFood Analytical Methods$gv.14, 2021.
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Registro original: |
Embrapa Pecuária Sudeste (CPPSE) |
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Registro Completo
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Biblioteca(s): |
Embrapa Agroindústria Tropical. |
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Data corrente: |
04/11/2009 |
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Data da última atualização: |
16/06/2017 |
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Tipo da produção científica: |
Artigo em Anais de Congresso / Nota Técnica |
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Autoria: |
AGUIAR, A. E. X.; CRUZ, M. L. B. da; FUCK JUNIOR, S. C. de F. |
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Afiliação: |
Antônia Elisangela Ximenes Aguiar, UECE; Maria Lúcia Brito da Cruz, UECE; SERGIO CESAR DE FRANCA FUCK JUNIOR, CNPAT. |
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Título: |
Sensoriamento Remoto aplicado à Apicultura de Mombaça-CE: uma alternativa conservacionista nas atividades rurais. |
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Ano de publicação: |
2009 |
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Fonte/Imprenta: |
In: SIMPÓSIO BRASILEIRO DE GEOGRAFIA FÍSICA APLICADA, 13., 2009, Viçosa-MG. Anais... Viçosa-MG: Universidade Federal de Viçosa, 2009. |
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Idioma: |
Português |
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Palavras-Chave: |
Mapeamento de florados. |
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Thesagro: |
Apicultura; Sensoriamento Remoto. |
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Categoria do assunto: |
-- |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/CNPAT-2010/11391/1/AT09002.pdf
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Marc: |
LEADER 00619nam a2200157 a 4500
001 1573993
005 2017-06-16
008 2009 bl uuuu u00u1 u #d
100 1 $aAGUIAR, A. E. X.
245 $aSensoriamento Remoto aplicado à Apicultura de Mombaça-CE$buma alternativa conservacionista nas atividades rurais.
260 $aIn: SIMPÓSIO BRASILEIRO DE GEOGRAFIA FÍSICA APLICADA, 13., 2009, Viçosa-MG. Anais... Viçosa-MG: Universidade Federal de Viçosa$c2009
650 $aApicultura
650 $aSensoriamento Remoto
653 $aMapeamento de florados
700 1 $aCRUZ, M. L. B. da
700 1 $aFUCK JUNIOR, S. C. de F.
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Embrapa Agroindústria Tropical (CNPAT) |
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