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 | Acesso ao texto completo restrito à biblioteca da Embrapa Agroindústria de Alimentos. Para informações adicionais entre em contato com ctaa.biblioteca@embrapa.br. |
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Registro Completo |
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Biblioteca(s): |
Embrapa Agroindústria de Alimentos. |
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Data corrente: |
31/08/2017 |
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Data da última atualização: |
31/08/2017 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
REGO, E. C. P. DO; GUIMARÃES, E. DE F.; RODRIGUES, J. M.; SCARLATO, R. C.; NOGUEIRA, R. I.; PEREIRA NETTO, A. D. |
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Afiliação: |
Eliane Cristina Pires do Rego, INMETRO; Evelyn de Freitas Guimarães, INMETRO; Janaína Marques Rodrigues, INMETRO; Renata Cristina Scarlato, INMETRO; REGINA ISABEL NOGUEIRA, CTAA; Annibal Duarte Pereira Netto, UFF. |
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Título: |
Feasibility study for development of candidate reference material for food analysis: Chloramphenicol in milk powder. |
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Ano de publicação: |
2017 |
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Fonte/Imprenta: |
Measurement, n. 98, p. 300-304, 2017. |
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Idioma: |
Inglês |
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Conteúdo: |
Reliable analytical results are necessary to ensure effective consumer protection and the use of certified reference material (CRM) is an important tool for quality assurance. The Brazilian Metrology Institute (Inmetro) studied the feasibility of the production of a candidate CRM of chloramphenicol (CAP) in milk. CAP is an antibiotic banned for treatment of food-producing animals. A minimum required performance limit (MRPL) for analytical methods of 0.3 lg kg1 was set by the European Community for the detection of CAP residues in food matrices. Liquid chromatography with isotope dilution mass spectrometry (LC? IDMS) was employed for CAP determination and water content was measured by Karl Fischer coulometric titration. The feasibility study showed milk powder processed with both spray dryer and lyophilization lead to the best results, showing good degree of inhomogeneity for CAP residues (5.0%) and for water content (3.0%), therefore demonstrating that the production of this candidate CRM was feasible |
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Palavras-Chave: |
Feasibility study; Homogeneity Certified Reference Material (CRM). |
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Thesaurus Nal: |
chloramphenicol; milk. |
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Categoria do assunto: |
X Pesquisa, Tecnologia e Engenharia |
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Marc: |
LEADER 01741naa a2200229 a 4500
001 2074788
005 2017-08-31
008 2017 bl uuuu u00u1 u #d
100 1 $aREGO, E. C. P. DO
245 $aFeasibility study for development of candidate reference material for food analysis$bChloramphenicol in milk powder.$h[electronic resource]
260 $c2017
520 $aReliable analytical results are necessary to ensure effective consumer protection and the use of certified reference material (CRM) is an important tool for quality assurance. The Brazilian Metrology Institute (Inmetro) studied the feasibility of the production of a candidate CRM of chloramphenicol (CAP) in milk. CAP is an antibiotic banned for treatment of food-producing animals. A minimum required performance limit (MRPL) for analytical methods of 0.3 lg kg1 was set by the European Community for the detection of CAP residues in food matrices. Liquid chromatography with isotope dilution mass spectrometry (LC? IDMS) was employed for CAP determination and water content was measured by Karl Fischer coulometric titration. The feasibility study showed milk powder processed with both spray dryer and lyophilization lead to the best results, showing good degree of inhomogeneity for CAP residues (5.0%) and for water content (3.0%), therefore demonstrating that the production of this candidate CRM was feasible
650 $achloramphenicol
650 $amilk
653 $aFeasibility study
653 $aHomogeneity Certified Reference Material (CRM)
700 1 $aGUIMARÃES, E. DE F.
700 1 $aRODRIGUES, J. M.
700 1 $aSCARLATO, R. C.
700 1 $aNOGUEIRA, R. I.
700 1 $aPEREIRA NETTO, A. D.
773 $tMeasurement$gn. 98, p. 300-304, 2017.
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Registro original: |
Embrapa Agroindústria de Alimentos (CTAA) |
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| Registros recuperados : 10 | |
| 7. |  | LEMOS, M. A. T.; MATOS, C. A.; RESENDE, M. F. de; PRADO, R. B.; DONAGEMMA, R. A.; PEREIRA NETTO, A. D. Development, validation, and application of a method for selected avermectin determination in rural waters using high performance liquid chromatography and fluorescence detection. Ecotoxicology and Environmental Safety, v. 133, p. 424-432, Nov. 2016.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 2 |
| Biblioteca(s): Embrapa Solos. |
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| 8. | | ROCHA, D. A. M.; TORRES, J. P. M.; REICHEL, K.; NOVOTNY, E. H.; ESTRELLA, L. F.; MEDEIROS, R. O.; PEREIRA NETTO, A. D. Determination of polychlorinated dibenzo-p-dioxins and dibenzofurans (PCDD/Fs) in Brazilian cow milk. Science of the Total Environment, v. 572, p. 177-184, Dec. 2016.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 1 |
| Biblioteca(s): Embrapa Solos. |
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| 9. | | SILVA, M. C. Da; CASTRO, E. da S. G. de; BARRETO, J. do N.; MARTINS, P. V. de O.; SILVA, G. L. da; SILVA, R. F. da; SANTOS, D. G. dos; FREITAS-SILVA, O.; SIMÃO, J. B. P.; SILVA JUNIOR, A. I. da S.; PEREIRA NETTO, A. D. Evaluation of ochratoxin A in specialty fermented coffees produced in Pedra Menina, Caparaó region (MG and ES), Brazil. In: REUNIÃO ANUAL DA SBQ, 45., 2022, Maceió. Química para o desenvolvimento sustentável e soberano: anais. Maceió: Aptor Software, 2022. p. 157.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| 10. | | SILVA, M. C. DA; CASTRO, E. DA S. G. DE; BARRETO, J. DO N.; MARTINS, P. V. DE O.; SILVA, G. L. DA; SILVA, R. F. DA; SANTOS, D. G. DOS; FREITAS-SILVA, O.; SIMÃO, J. B. P.; SILVA JUNIOR, A. I. DA; PEREIRA NETTO, A. D. Ochratoxin a levels in fermented specialty coffees from Caparaó, Brazil: Is it a cause of concern for coffee drinkers? Food Additives & Contaminants: Part A, ago., 2021. 11 p.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: A - 2 |
| Biblioteca(s): Embrapa Agroindústria de Alimentos. |
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| Registros recuperados : 10 | |
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| Nenhum registro encontrado para a expressão de busca informada. |
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