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1. | | BRUSKIEWICH, R.; SENGER, M.; DAVENPORT, G.; RUIZ, M.; ROUARD, M.; HAZEKAMP, T.; TAKEYA, M.; DOI, K.; SATOH, K.; COSTA, M.; SIMON, R.; BALAJI, J.; AKINTUNDE, A.; MAULEON, R.; WANCHANA, S.; SHAH, T.; ANACLETO, M.; PORTUGAL, A.; ULAT, V. J.; THONGJUEA, S.; BRAAK, K.; RITTER, S.; DEREEPER, M.; SKOFIC, M.; ROJAS, E.; MARTINS, N.; PAPPAS, G.; ALAMBAN, R.; ALMODIEL, R.; BARBOZA, L. H.; DETRAS, J.; MANANSALA, K.; MENDOZA, M. J.; MORALES, J.; PERALTA, B.; VALERIO, R.; ZHANG, Y.; GREGORIO, S.; HERMOCILLA, J.; ECHAVEZ, M.; YAP, J. M.; FARMER, A.; SCHILTZ, G.; LEE, J.; CASSTEVENS, T.; JAISWAL, P.; MEINTJES, A.; WILKINSON, M.; GOOD, B.; WAGNER, J.; MORRIS, J.; MARSHALL, D.; COLLINS, A.; KIKUCHI, S.; METZ, T.; MCLAREN, G.; HINTUM, T. van. The generation challenge programme platform: semantic standards and workbench for crop science. International Journal of Plant Genomics, v.2008, 6 p., 2008. doi:10.1155/2008/369601. Biblioteca(s): Embrapa Recursos Genéticos e Biotecnologia. |
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Registro Completo
Biblioteca(s): |
Embrapa Meio Ambiente. |
Data corrente: |
03/09/2012 |
Data da última atualização: |
20/12/2012 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 2 |
Autoria: |
HASHIMOTO, J. C.; PASCHOAL, J. A. R.; QUEIROZ, S. C. do N. de; FERRACINI, V. L.; ASSALIN, M. R.; REYES, F. G. R. |
Afiliação: |
JULIANA CAMPOS HASHIMOTO, UNICAMP; JONAS AUGUSTO RIZZATO PASCHOAL, UNICAMP; SONIA CLAUDIA DO N DE QUEIROZ, CNPMA; VERA LUCIA FERRACINI, CNPMA; MARCIA REGINA ASSALIN, CNPMA; FELIX GUILLERMO REYES REYES, UNICAMP. |
Título: |
A simple method for the determination of malachite green and leucomalachite green residues in fish by a modified QuEChERS extraction and LC/MS/MS. |
Ano de publicação: |
2012 |
Fonte/Imprenta: |
Journal of AOAC International, Arlington, v. 95, n. 3, p. 913-922, 2012. |
Idioma: |
Inglês |
Conteúdo: |
A simple method using HPLC/MS/MS was developed and validated to determine residues of malachite green (MG) and leucomalachite green (LMG) in fish fillet. A modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) technique was used to perform the sample preparation. The optimal extraction and cleanup conditions were established using an experimental design. The validation parameters obtained to determine both MG and LMG complied with the requirements established by regulatory agencies for the presence of such substances in fish, which establish that the method must attain, at least, a minimum required performance limit of 2 ng/g. The accuracy values ranged etween 95 and 107%, and the precision values were lower than 11.2%. The method was used in the analysis of tilapia samples (n = 20) commercialized in Campinas, SP, Brazil. None of the samples presented detectable levels of MG or LMG residues. |
Thesagro: |
Análise química; Cromatografia; Resíduo químico; Tilápia; Toxicologia de alimento. |
Thesaurus NAL: |
Chemical residues; Liquid chromatography; Mass spectrometry; Tilapia (Cichlidae). |
Categoria do assunto: |
H Saúde e Patologia |
Marc: |
LEADER 01862naa a2200289 a 4500 001 1932815 005 2012-12-20 008 2012 bl uuuu u00u1 u #d 100 1 $aHASHIMOTO, J. C. 245 $aA simple method for the determination of malachite green and leucomalachite green residues in fish by a modified QuEChERS extraction and LC/MS/MS.$h[electronic resource] 260 $c2012 520 $aA simple method using HPLC/MS/MS was developed and validated to determine residues of malachite green (MG) and leucomalachite green (LMG) in fish fillet. A modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) technique was used to perform the sample preparation. The optimal extraction and cleanup conditions were established using an experimental design. The validation parameters obtained to determine both MG and LMG complied with the requirements established by regulatory agencies for the presence of such substances in fish, which establish that the method must attain, at least, a minimum required performance limit of 2 ng/g. The accuracy values ranged etween 95 and 107%, and the precision values were lower than 11.2%. The method was used in the analysis of tilapia samples (n = 20) commercialized in Campinas, SP, Brazil. None of the samples presented detectable levels of MG or LMG residues. 650 $aChemical residues 650 $aLiquid chromatography 650 $aMass spectrometry 650 $aTilapia (Cichlidae) 650 $aAnálise química 650 $aCromatografia 650 $aResíduo químico 650 $aTilápia 650 $aToxicologia de alimento 700 1 $aPASCHOAL, J. A. R. 700 1 $aQUEIROZ, S. C. do N. de 700 1 $aFERRACINI, V. L. 700 1 $aASSALIN, M. R. 700 1 $aREYES, F. G. R. 773 $tJournal of AOAC International, Arlington$gv. 95, n. 3, p. 913-922, 2012.
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Embrapa Meio Ambiente (CNPMA) |
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