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Registro Completo |
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Biblioteca(s): |
Embrapa Semiárido; Embrapa Uva e Vinho. |
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Data corrente: |
17/09/2013 |
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Data da última atualização: |
25/04/2017 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Autoria: |
NATIVIDADE, M. M. P.; CORREA, L. C.; SOUZA, S. V. C. de; PEREIRA, G. E.; LIMA, L. C. de O. |
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Afiliação: |
MARIANA MIRELLE PEREIRA NATIVIDADE, Universidade Federal de Lavras; LUIZ CLAUDIO CORREA, CPATSA; SCHEILLA VITORINO CARVALHO DE SOUZA, Universidade Federal de Minas Gerais; GIULIANO ELIAS PEREIRA, CNPUV / CPATSA; LUIZ CARLOS DE OLIVEIRA LIMA, Universidade Federal de Lavras. |
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Título: |
Simultaneous analysis of 25 phenolic compounds in grape juice for HPLC: Method validation and characterization of São Francisco Valley samples. |
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Ano de publicação: |
2013 |
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Fonte/Imprenta: |
Microchemical Journal, New York, v. 110, p. 665-674, abr. 2013. |
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Idioma: |
Inglês |
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Conteúdo: |
A HPLCmethod for simultaneous determination of 25 phenolic compounds in grape juicewas optimized, validated and applied in the characterization of juices produced in São Francisco Valley (SFV), Brazil. The performance characteristics of the method were established by assays with standard solutions of phenolic compounds, spiked and unspiked samples. Linearity,matrix effects, trueness, precision, detection and quantification limits were evaluated. Linearity was demonstrated in the concentration ranges tested for all phenolic compounds. Significant matrix effects were not identified for the studied compounds.Mean recoveries ranged from86.18 to 106.50%, demonstrating no lack of trueness. Precision of the method was confirmed for the 25 phenolic compounds, with acceptable repeatability relative standard deviations (from 0.71 to 9.24%) and within-reproducibility relative standard deviations (from1.34 to 9.26%) for unspiked and spiked samples. The theoretical limits of detection and quantification of themethod varied from 0.001 to 0.19 Mg mL-1 and 0.003 to 0.37 Mg mL-1, respectively. The results of the validation process showed that the proposed method is fitness for purpose. This method was able to identify simultaneously 25 phenolic compounds and had advantages such as low consumption of solvents and easy sample preparation. The phenolic profile of the grape juices from SFV varied according the grape cultivar. Phenolics of the anthocyanins and tannins class predominated in red grape juices, while in white grape juice phenolic acids and tannins were found at high concentrations. MenosA HPLCmethod for simultaneous determination of 25 phenolic compounds in grape juicewas optimized, validated and applied in the characterization of juices produced in São Francisco Valley (SFV), Brazil. The performance characteristics of the method were established by assays with standard solutions of phenolic compounds, spiked and unspiked samples. Linearity,matrix effects, trueness, precision, detection and quantification limits were evaluated. Linearity was demonstrated in the concentration ranges tested for all phenolic compounds. Significant matrix effects were not identified for the studied compounds.Mean recoveries ranged from86.18 to 106.50%, demonstrating no lack of trueness. Precision of the method was confirmed for the 25 phenolic compounds, with acceptable repeatability relative standard deviations (from 0.71 to 9.24%) and within-reproducibility relative standard deviations (from1.34 to 9.26%) for unspiked and spiked samples. The theoretical limits of detection and quantification of themethod varied from 0.001 to 0.19 Mg mL-1 and 0.003 to 0.37 Mg mL-1, respectively. The results of the validation process showed that the proposed method is fitness for purpose. This method was able to identify simultaneously 25 phenolic compounds and had advantages such as low consumption of solvents and easy sample preparation. The phenolic profile of the grape juices from SFV varied according the grape cultivar. Phenolics of the anthocyanins and tannins class predominated in red gr... Mostrar Tudo |
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Palavras-Chave: |
Composto fenológico; HPLC; Perfil fenólico; Suco de uva; Vale do São Francisco. |
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Thesagro: |
Suco; Uva; Viticultura. |
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Thesaurus Nal: |
Grapes. |
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Categoria do assunto: |
F Plantas e Produtos de Origem Vegetal |
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URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/89541/1/Mariana-Pereira-et-al-MJ-092013.pdf
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/95257/1/Mariana-Pereira-et-al-MJ-092013.pdf
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Marc: |
LEADER 02441naa a2200277 a 4500
001 1966365
005 2017-04-25
008 2013 bl uuuu u00u1 u #d
100 1 $aNATIVIDADE, M. M. P.
245 $aSimultaneous analysis of 25 phenolic compounds in grape juice for HPLC$bMethod validation and characterization of São Francisco Valley samples.$h[electronic resource]
260 $c2013
520 $aA HPLCmethod for simultaneous determination of 25 phenolic compounds in grape juicewas optimized, validated and applied in the characterization of juices produced in São Francisco Valley (SFV), Brazil. The performance characteristics of the method were established by assays with standard solutions of phenolic compounds, spiked and unspiked samples. Linearity,matrix effects, trueness, precision, detection and quantification limits were evaluated. Linearity was demonstrated in the concentration ranges tested for all phenolic compounds. Significant matrix effects were not identified for the studied compounds.Mean recoveries ranged from86.18 to 106.50%, demonstrating no lack of trueness. Precision of the method was confirmed for the 25 phenolic compounds, with acceptable repeatability relative standard deviations (from 0.71 to 9.24%) and within-reproducibility relative standard deviations (from1.34 to 9.26%) for unspiked and spiked samples. The theoretical limits of detection and quantification of themethod varied from 0.001 to 0.19 Mg mL-1 and 0.003 to 0.37 Mg mL-1, respectively. The results of the validation process showed that the proposed method is fitness for purpose. This method was able to identify simultaneously 25 phenolic compounds and had advantages such as low consumption of solvents and easy sample preparation. The phenolic profile of the grape juices from SFV varied according the grape cultivar. Phenolics of the anthocyanins and tannins class predominated in red grape juices, while in white grape juice phenolic acids and tannins were found at high concentrations.
650 $aGrapes
650 $aSuco
650 $aUva
650 $aViticultura
653 $aComposto fenológico
653 $aHPLC
653 $aPerfil fenólico
653 $aSuco de uva
653 $aVale do São Francisco
700 1 $aCORREA, L. C.
700 1 $aSOUZA, S. V. C. de
700 1 $aPEREIRA, G. E.
700 1 $aLIMA, L. C. de O.
773 $tMicrochemical Journal, New York$gv. 110, p. 665-674, abr. 2013.
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Esconder MarcMostrar Marc Completo |
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Registro original: |
Embrapa Semiárido (CPATSA) |
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| Registros recuperados : 76 | |
| 23. |  | CORREA, L. C.; BIASOTO, A. C. T.; SILVA, P. T. de S. e; PEREIRA, G. E.; RYBKA, A. C. P. Development and validation of methodology for the determination of sugars in must, grape juice and different types of wine. In: WORLD CONGRESS OF FOOD SCIENCE AND TECHNOLOGY, 16.; LATIN AMERICAN SEMINAR OF FOOD SCIENCE AND TECHNOLOGY, 17., 2012, Foz do Iguaçu. Addressing global food security and wellness through food science and technology: abstracts. Foz do Iguaçu: ALACCTA, 2012. 1 CD-ROM.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido; Embrapa Uva e Vinho. |
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| 24. | | CARVALHO, E. S. S. de; BIASOTO, A. C. T.; CORREA, L. C.; LIMA, M. A. C. de; DRUZIAN, J. I. Influência do tempo de maceração na composição físico-química, fenólica e coloração do vinho tinto Touriga nacional produzido no Submédio do Vale do São Francisco. In: ENCONTRO NACIONAL DA AGROINDÚSTRIA, 4., 2018, Bananeiras. Anais... Bananeiras: UFPB: CABA, 2018.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 25. | | BIASOTO, A. C. T.; CORREA, L. C.; PEREIRA, G. E.; OLIVEIRA, J. B.; MENEZES, T. R.; RYBKA, A. C. P. Influência do estádio de maturação da uva e tempo de duração da maceração sobre a estabilidade fenólica do vinho tinto tropical elaborado no Vale do São Francisco. In: CONGRESSO LATINO-AMERICANO DE VITICULTURA E ENOLOGIA, 15.; CONGRESSO BRASILEIRO DE VITICULTURA E ENOLOGIA, 13., 2015, Bento Gonçalves. Resumos... Bento Gonçalves: Embrapa Uva e Vinho: Associação Brasileira de Enologia, 2015. 1 Pen drive.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido; Embrapa Uva e Vinho. |
| |
| 26. | | PADILHA, C. V. da S.; BIASOTO, A. C. T.; CORREA, L. C.; LIMA, M. dos S.; PEREIRA, G. E. Phenolic compounds and antioxidant activity of commercial tropical red wines (Vitis vinifera) from the São Francisco Valley, Brazil. In: INTERNATIONAL SYMPOSIUM ON TROPICAL WINES, 5., 2016, Petrolina. Book of abstracts... Petrolina: Embrapa Semiárido, 2016. p. 58.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 28. | | BARBARÁ, J. A.; NICOLLI, K. P.; BIASOTO, A. C. T.; SILVA E. A. S.; CORREA, L. C.; ZINI, C. A. Phenolic content, physical-chemical composition and antioxidant activity of Syrah wines elaborated in São Francisco Valley during ripening. In: WORLD VINE AND WINE CONGRESS, 39.; GENERAL ASSEMBLY OF THE OIV, 14., 2016, Bento Gonçalves. Vitiviniculture: technological advances to market challenges: abstracts. Bento Gonçalves: International Organisation of Vine and Wine, 2016. 1 Pen drive.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 30. | | SILVA, L. T.; SILVA, E. de O.; FIGUEIREDO, M. C. B. de; CORREA, L. C.; ARAGAO, F. A. S. de. Pós-colheita do melão amarelo "goldex" cultivado sob adubação verde e plantio direto com diferentes coberturas. Irriga, Botucatu, v. 21, n. 4, p. 764-778, 2016.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: B - 1 |
| Biblioteca(s): Embrapa Agroindústria Tropical; Embrapa Semiárido. |
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| 31. | | CORRÊA, L. C.; SANTOS, C. A. F.; LIMA, G. P. P.; RODRIGUES, M. A.; COSTA, T. P. P. Similaridade genética entre acessos de goiabeiras e araçazeiros baseada em marcadores moleculares AFLP. Revista Brasileira de Fruticultura, Jaboticabal, v. 33, n. 3, p. 859-867, 2011.| Tipo: Artigo em Periódico Indexado | Circulação/Nível: B - 1 |
| Biblioteca(s): Embrapa Semiárido. |
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| 34. | | SANTOS, C. A. F.; CORREA, L. C.; RIBEIRO, H. L. C.; OLIVEIRA, M. M. de; ARAÚJO, J. S. Transferência de primers SSRs de Allium fistulosum para A. cepa. Horticultura Brasileira, Brasília, DF, v. 27, n. 2, p. S3419-3422, ago. 2009. 1 CD-ROM. Suplemento. Edição dos Trabalhos do 49 Congresso Brasileiro de Olericultura, Águas de Lindóia, ago. 2009.| Tipo: Artigo em Anais de Congresso / Nota Técnica |
| Biblioteca(s): Embrapa Semiárido. |
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| 35. | | SILVA, I. S.; BARROS, A. P. A.; SILVA, A. de S.; NOGUEIRA, E. T. da; CORREA, L. C.; BIASOTO, A. C. T. Avaliação da composição fenólica de vinhos brancos "chenin blanc" elaborados com diferentes agentes de colagem. In: ENCONTRO NACIONAL DA AGROINDÚSTRIA, 4., 2018, Bananeiras. Anais... Bananeiras: UFPB: CABA, 2018.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 36. | | PADILHA, C. V. S.; BIASOTO, A. C. T.; CORREA, L. C.; LIMA, M. S.; BORDIGNON-LUIZ, M. T.; PEREIRA, G. E. Anthocyanin composition of young red wine cv. Ruby Cabernet and Syrah: effect of time and storage conditions. In: CONGRESSO LATINO-AMERICANO DE VITICULTURA E ENOLOGIA, 15.; CONGRESSO BRASILEIRO DE VITICULTURA E ENOLOGIA, 13., 2015, Bento Gonçalves. Resumos... Bento Gonçalves: Embrapa Uva e Vinho: Associação Brasileira de Enologia, 2015. 1 Pen drive.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido; Embrapa Uva e Vinho. |
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| 37. | | OLIVEIRA, W. P. de; CORREA, L. C.; MIRANDA, M. S.; CAMARGO, A. C. de; LIMA, M. A. C. de; BIASOTO, A. C. T. Compartive phenolic profile and antiradical activity of syrah wine and its manufature by-products. In: WORLD VINE AND WINE CONGRESS, 39.; GENERAL ASSEMBLY OF THE OIV, 14., 2016, Bento Gonçalves. Vitiviniculture: technological advances to market challenges: abstracts. Bento Gonçalves: International Organisation of Vine and Wine, 2016. 1 Pen drive.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 38. | | FONSECA, J. M. S. de S.; BONFIM, W. M. D.; ANDRADE NETO, E. R. de; CORREA, L. C.; LIMA, M. A. C. de. Características físico-químicas e quantificação de compostos fenólicos em frutos de acessos de umbuzeiro. In: JORNADA DE INICIAÇÃO CIENTÍFICA DA EMBRAPA SEMIÁRIDO, 14., 2019, Petrolina. Anais... Petrolina: Embrapa Semiárido, 2019. p. 143-148. (Embrapa Semiárido. Documentos, 288).| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 39. | | BARBARÁ, J. A.; BIASOTO, A. C. T.; NICOLLI, K. P.; QUEIROZ, L. B.; SILVA, E. A. S.; CORREA, L. C.; WELKE, J. E.; ZINI, C. A. Evaluating the typicality of the aroma of Syrah tropical wines from the Sub-middle São Francisco Valley employing gas chromatography coupled to olfactometry detection (GC-O). In: CONGRESSO LATINO-AMERICANO DE VITICULTURA E ENOLOGIA, 15.; CONGRESSO BRASILEIRO DE VITICULTURA E ENOLOGIA, 13., 2015, Bento Gonçalves. Resumos... Bento Gonçalves: Embrapa Uva e Vinho: Associação Brasileira de Enologia, 2015. 1 Pen drive.| Tipo: Resumo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| 40. | | OLIVEIRA, W. P.; CORREA, L. C.; BARROS, P. A.; RIBEIRO T. P.; SILVA, D. J.; LIMA, M. A. C. de; MIRANDA, M. S.; BIASOTO, A. C. T. Caracterização de subprodutos da vinificação (borra e engaço) com relação ao teor de antocianinas, fenólicos totais e atividade antioxidante. In: ENCONTRO NACIONAL DE ANALISTAS DE ALIMENTOS, 19.; CONGRESSO LATINO-AMERICANO DE ANALISTAS DE ALIMENTOS, 5., 2015, Natal. Desafios analíticos e segurança alimentar. Natal: LACEN-RN: SESAP: UFRN, 2015. 1 CD-ROM.| Tipo: Artigo em Anais de Congresso |
| Biblioteca(s): Embrapa Semiárido. |
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| Registros recuperados : 76 | |
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| Nenhum registro encontrado para a expressão de busca informada. |
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